Efficient 18.8 T MAS-DNP NMR reveals hidden side chains in amyloid fibrils

Dynamic Nuclear Polarization for Sensitivity Enhancement in Biomolecular Solid-State NMR

(2022) Thomas Biedenbänder et al.   CHEMICAL REVIEWS

Efficient Pulsed Dynamic Nuclear Polarization with the X-Inverse-X Sequence

(2022) Venkata SubbaRao Redrouthu et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Probing Watson-Crick and Hoogsteen base pairing in duplex DNA using dynamic nuclear polarization solid-state NMR spectroscopy

(2022) Daniel W. Conroy et al.   PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA

Designing broadband pulsed dynamic nuclear polarization sequences in static solids

(2022) Nino Wili et al.   Science Advances

Observing Nearby Nuclei on Paramagnetic Trityls and MOFs via DNP and Electron Decoupling

(2022) Kong Ooi Tan et al.   CHEMISTRY-A EUROPEAN JOURNAL

Application of DNP-enhanced solid-state NMR to studies of amyloid-β peptide interaction with lipid membranes

(2021) Thomas Deo et al.   CHEMISTRY AND PHYSICS OF LIPIDS

Structures of Pathological and Functional Amyloids and Prions, a Solid-State NMR Perspective

(2021) Asen Daskalov et al.   Frontiers in Molecular Neuroscience

Solid-state MAS NMR at ultra low temperature of hydrated alanine doped with DNP radicals

(2021) Yuanxin Li et al.   JOURNAL OF MAGNETIC RESONANCE

Efficient Dynamic Nuclear Polarization up to 230 K with Hybrid BDPA-Nitroxide Radicals at a High Magnetic Field

(2021) Georges Menzildjian et al.   JOURNAL OF PHYSICAL CHEMISTRY B

Overhauser Dynamic Nuclear Polarization with Selectively Deuterated BDPA Radicals

(2021) Léo Delage-Laurin et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

1H detection and dynamic nuclear polarization–enhanced NMR of Aβ1-42 fibrils

(2021) Salima Bahri et al.   PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA

Advances in studying protein disorder with solid-state NMR

(2020) Ansgar B. Siemer   SOLID STATE NUCLEAR MAGNETIC RESONANCE

Solid-state NMR of plant and fungal cell walls: A critical review

(2020) Wancheng Zhao et al.   SOLID STATE NUCLEAR MAGNETIC RESONANCE

Postmodification via Thiol-Click Chemistry Yields Hydrophilic Trityl-Nitroxide Biradicals for Biomolecular High-Field Dynamic Nuclear Polarization

(2020) Weixiang Zhai et al.   JOURNAL OF PHYSICAL CHEMISTRY B

Dynamic Nuclear Polarization Enhancement of 200 at 21.15 T Enabled by 65 kHz Magic Angle Spinning

(2020) Pierrick Berruyer et al.   Journal of Physical Chemistry Letters

Dimer Organization of Membrane‐Associated NS5A of Hepatitis C Virus as Determined by Highly Sensitive 1 H‐Detected Solid‐State NMR

(2020) Vlastimil Jirasko et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Time-optimized pulsed dynamic nuclear polarization

(2019) Kong Ooi Tan et al.   Science Advances

Improved waveguide coupling for 1.3 mm MAS DNP probes at 263 GHz

(2019) Armin Purea et al.   JOURNAL OF MAGNETIC RESONANCE

Recent developments in MAS DNP-NMR of materials

(2019) Andrew Rankin et al.   SOLID STATE NUCLEAR MAGNETIC RESONANCE

The Amyloid Phenomenon and Its Significance in Biology and Medicine

(2019) Christopher M. Dobson et al.   Cold Spring Harbor Perspectives in Biology

Two decades of progress in structural and dynamic studies of amyloids by solid-state NMR

(2019) Christopher P. Jaroniec   JOURNAL OF MAGNETIC RESONANCE

Aromatic Ring Dynamics, Thermal Activation, and Transient Conformations of a 468 kDa Enzyme by Specific 1H–13C Labeling and Fast Magic-Angle Spinning NMR

(2019) Diego F. Gauto et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Cryo-EM of amyloid fibrils and cellular aggregates

(2019) Anthony WP Fitzpatrick et al.   CURRENT OPINION IN STRUCTURAL BIOLOGY

Dynamic Nuclear Polarization-Enhanced Biomolecular NMR Spectroscopy at High Magnetic Field with Fast Magic-Angle Spinning

(2018) Kristaps Jaudzems et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Structural Studies of Self-Assembled Subviral Particles: Combining Cell-Free Expression with 110 kHz MAS NMR Spectroscopy

(2018) Guillaume David et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Magic angle spinning NMR below 6 K with a computational fluid dynamics analysis of fluid flow and temperature gradients

(2018) Erika L. Sesti et al.   JOURNAL OF MAGNETIC RESONANCE

3D structure determination of amyloid fibrils using solid-state NMR spectroscopy

(2018) Antoine Loquet et al.   METHODS

Functional Amyloids in Health and Disease

(2018) Antoine Loquet et al.   JOURNAL OF MOLECULAR BIOLOGY

DNP NMR of Biomolecular Assemblies

(2018) Kristaps Jaudzems et al.   JOURNAL OF STRUCTURAL BIOLOGY

BDPA-Nitroxide Biradicals Tailored for Efficient Dynamic Nuclear Polarization Enhanced Solid-State NMR at Magnetic Fields up to 21.1 T

(2018) Dorothea Wisser et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Line-Broadening in Low-Temperature Solid-State NMR Spectra of Fibrils

(2017) Thomas Bauer et al.   JOURNAL OF BIOMOLECULAR NMR

Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR

(2017) Qing Zhe Ni et al.   JOURNAL OF PHYSICAL CHEMISTRY B

Proton-Assisted Recoupling (PAR) in Peptides and Proteins

(2017) Kevin J. Donovan et al.   JOURNAL OF PHYSICAL CHEMISTRY B

3D MAS NMR Experiment Utilizing Through-Space 15N–15N Correlations

(2017) Kevin J. Donovan et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Combining DNP NMR with segmental and specific labeling to study a yeast prion protein strain that is not parallel in-register

(2017) Kendra K. Frederick et al.   PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA

Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR

(2017) Aany Sofia Lilly Thankamony et al.   PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY

Insights into protein misfolding and aggregation enabled by solid-state NMR spectroscopy

(2017) Patrick C.A. van der Wel   SOLID STATE NUCLEAR MAGNETIC RESONANCE

Solid-state NMR sequential assignment of an Amyloid-β(1–42) fibril polymorph

(2016) Francesco Ravotti et al.   Biomolecular NMR Assignments

Surface Binding of TOTAPOL Assists Structural Investigations of Amyloid Fibrils by Dynamic Nuclear Polarization NMR Spectroscopy

(2016) Madhu Nagaraj et al.   CHEMBIOCHEM

High resolution observed in 800 MHz DNP spectra of extremely rigid type III secretion needles

(2016) Pascal Fricke et al.   JOURNAL OF BIOMOLECULAR NMR

Advanced instrumentation for DNP-enhanced MAS NMR for higher magnetic fields and lower temperatures

(2016) Yoh Matsuki et al.   JOURNAL OF MAGNETIC RESONANCE

Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning

(2016) Kent Thurber et al.   JOURNAL OF MAGNETIC RESONANCE

Atomic Resolution Structure of Monomorphic Aβ42 Amyloid Fibrils

(2016) Michael T. Colvin et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Efficient Dynamic Nuclear Polarization at 800 MHz/527 GHz with Trityl-Nitroxide Biradicals

(2015) Guinevere Mathies et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Magic Angle Spinning NMR of Proteins: High-Frequency Dynamic Nuclear Polarization and1H Detection

(2015) Yongchao Su et al.   Annual Review of Biochemistry

Solid-state NMR sequential assignments of the N-terminal domain of HpDnaB helicase

(2015) Thomas Wiegand et al.   Biomolecular NMR Assignments

The structure of fibrils from ‘misfolded’ proteins

(2015) Beat H Meier et al.   CURRENT OPINION IN STRUCTURAL BIOLOGY

Successive Stages of Amyloid-β Self-Assembly Characterized by Solid-State Nuclear Magnetic Resonance with Dynamic Nuclear Polarization

(2015) Alexey Potapov et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Visualizing Specific Cross-Protomer Interactions in the Homo-Oligomeric Membrane Protein Proteorhodopsin by Dynamic-Nuclear-Polarization-Enhanced Solid-State NMR

(2015) Jakob Maciejko et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

High Resolution Structural Characterization of Aβ42 Amyloid Fibrils by Magic Angle Spinning NMR

(2015) Michael T. Colvin et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Signal Transduction by a Fungal NOD-Like Receptor Based on Propagation of a Prion Amyloid Fold

(2015) Asen Daskalov et al.   PLOS BIOLOGY

Amplifying Dynamic Nuclear Polarization of Frozen Solutions by Incorporating Dielectric Particles

(2014) Dominik J. Kubicki et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Physical and structural basis for polymorphism in amyloid fibrils

(2014) Robert Tycko   PROTEIN SCIENCE

Highly Efficient, Water-Soluble Polarizing Agents for Dynamic Nuclear Polarization at High Frequency

(2013) Claire Sauvée et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Yet another polymorph of α-synuclein: solid-state sequential assignments

(2013) Julia Gath et al.   Biomolecular NMR Assignments

Matrix-free dynamic nuclear polarization enables solid-state NMR 13C–13C correlation spectroscopy of proteins at natural isotopic abundance

(2013) Hiroki Takahashi et al.   CHEMICAL COMMUNICATIONS

Studies on the MxiH Protein in T3SS Needles Using DNP-Enhanced ssNMR Spectroscopy

(2013) Pascal Fricke et al.   CHEMPHYSCHEM

Cryogenic solid state NMR studies of fibrils of the Alzheimer’s disease amyloid-β peptide: perspectives for DNP

(2013) Juan-Miguel Lopez del Amo et al.   JOURNAL OF BIOMOLECULAR NMR

Paramagnet induced signal quenching in MAS–DNP experiments in frozen homogeneous solutions

(2013) Björn Corzilius et al.   JOURNAL OF MAGNETIC RESONANCE

Higher Order Amyloid Fibril Structure by MAS NMR and DNP Spectroscopy

(2013) Galia T. Debelouchina et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Characterization of Stratum Corneum Molecular Dynamics by Natural-Abundance 13C Solid-State NMR

(2013) Sebastian Björklund et al.   PLoS One

Atomic structure and hierarchical assembly of a cross-  amyloid fibril

(2013) A. W. P. Fitzpatrick et al.   PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA

High-Temperature Dynamic Nuclear Polarization Enhanced Magic-Angle-Spinning NMR

(2012) Ümit Akbey et al.   APPLIED MAGNETIC RESONANCE

Atomic model of the type III secretion system needle

(2012) Antoine Loquet et al.   NATURE

Heteronuclear proton assisted recoupling

(2011) Gaël De Paëpe et al.   JOURNAL OF CHEMICAL PHYSICS

Intermolecular Structure Determination of Amyloid Fibrils with Magic-Angle Spinning and Dynamic Nuclear Polarization NMR

(2011) Marvin J. Bayro et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Low-temperature dynamic nuclear polarization at 9.4T with a 30mW microwave source

(2010) Kent R. Thurber et al.   JOURNAL OF MAGNETIC RESONANCE

Probing Water Accessibility in HET-s(218–289) Amyloid Fibrils by Solid-State NMR

(2010) Hélène Van Melckebeke et al.   JOURNAL OF MOLECULAR BIOLOGY

Atomic-Resolution Three-Dimensional Structure of HET-s(218−289) Amyloid Fibrils by Solid-State NMR Spectroscopy

(2010) Hélène Van Melckebeke et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Resolution and polarization distribution in cryogenic DNP/MAS experiments

(2010) Alexander B. Barnes et al.   PHYSICAL CHEMISTRY CHEMICAL PHYSICS

Cryogenic sample exchange NMR probe for magic angle spinning dynamic nuclear polarization

(2009) Alexander B. Barnes et al.   JOURNAL OF MAGNETIC RESONANCE

DNP enhanced frequency-selective TEDOR experiments in bacteriorhodopsin

(2009) Vikram S. Bajaj et al.   JOURNAL OF MAGNETIC RESONANCE

Functional Amyloids As Natural Storage of Peptide Hormones in Pituitary Secretory Granules

(2009) S. K. Maji et al.   SCIENCE

Solid-State NMR Reveals Structural Differences between Fibrils of Wild-Type and Disease-Related A53T Mutant α-Synuclein

(2008) Henrike Heise et al.   JOURNAL OF MOLECULAR BIOLOGY

Amyloid Fibrils of the HET-s(218-289) Prion Form a   Solenoid with a Triangular Hydrophobic Core

(2008) C. Wasmer et al.   SCIENCE