Limits of Resolution and Sensitivity of Proton Detected MAS Solid-State NMR Experiments at 111 kHz in Deuterated and Protonated Proteins

1 H-Detected Solid-State NMR Studies of Water-Inaccessible Proteins In Vitro and In Situ

(2016) João Medeiros-Silva et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

NMR Spectroscopic Assignment of Backbone and Side-Chain Protons in Fully Protonated Proteins: Microcrystals, Sedimented Assemblies, and Amyloid Fibrils

(2016) Jan Stanek et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Sensitive proton-detected solid-state NMR spectroscopy of large proteins with selective CH3 labelling: application to the 50S ribosome subunit

(2016) Vilius Kurauskas et al.   CHEMICAL COMMUNICATIONS

Atomic Resolution Structure of Monomorphic Aβ42 Amyloid Fibrils

(2016) Michael T. Colvin et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Solid-state NMR structure of a pathogenic fibril of full-length human α-synuclein

(2016) Marcus D Tuttle et al.   NATURE STRUCTURAL & MOLECULAR BIOLOGY

Structure of fully protonated proteins by proton-detected magic-angle spinning NMR

(2016) Loren B. Andreas et al.   PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA

Atomic-resolution structure of a disease-relevant Aβ(1–42) amyloid fibril

(2016) Marielle Aulikki Wälti et al.   PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA

Solid-state NMR structure of a pathogenic fibril of full-length human α-synuclein

(2016) Marcus D Tuttle et al.   NATURE STRUCTURAL & MOLECULAR BIOLOGY

Site-Specific Solid-State NMR Studies of “Trigger Factor” in Complex with the Large Ribosomal Subunit 50S

(2015) Emeline Barbet-Massin et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Protein resonance assignment at MAS frequencies approaching 100 kHz: a quantitative comparison of J-coupling and dipolar-coupling-based transfer methods

(2015) Susanne Penzel et al.   JOURNAL OF BIOMOLECULAR NMR

Spinning proteins, the faster, the better?

(2015) Anja Böckmann et al.   JOURNAL OF MAGNETIC RESONANCE

The chaperone αB-crystallin uses different interfaces to capture an amorphous and an amyloid client

(2015) Andi Mainz et al.   NATURE STRUCTURAL & MOLECULAR BIOLOGY

The chaperone αB-crystallin uses different interfaces to capture an amorphous and an amyloid client

(2015) Andi Mainz et al.   NATURE STRUCTURAL & MOLECULAR BIOLOGY

Nano-Mole Scale Side-Chain Signal Assignment by 1H-Detected Protein Solid-State NMR by Ultra-Fast Magic-Angle Spinning and Stereo-Array Isotope Labeling

(2015) Songlin Wang et al.   PLoS One

De Novo 3D Structure Determination from Sub-milligram Protein Samples by Solid-State 100 kHz MAS NMR Spectroscopy

(2014) Vipin Agarwal et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Proton Clouds to Measure Long-Range Contacts between Nonexchangeable Side Chain Protons in Solid-State NMR

(2014) Tessa Sinnige et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Rapid Proton-Detected NMR Assignment for Proteins with Fast Magic Angle Spinning

(2014) Emeline Barbet-Massin et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Proton-Detected Solid-State NMR Spectroscopy at Aliphatic Sites: Application to Crystalline Systems

(2013) Sam Asami et al.   ACCOUNTS OF CHEMICAL RESEARCH

Solid-state NMR spectroscopy structure determination of a lipid-embedded heptahelical membrane protein

(2013) Shenlin Wang et al.   NATURE METHODS

Optimal degree of protonation for 1H detection of aliphatic sites in randomly deuterated proteins as a function of the MAS frequency

(2012) Sam Asami et al.   JOURNAL OF BIOMOLECULAR NMR

Ultra-high resolution in MAS solid-state NMR of perdeuterated proteins: Implications for structure and dynamics

(2012) Bernd Reif   JOURNAL OF MAGNETIC RESONANCE

Atomic model of the type III secretion system needle

(2012) Antoine Loquet et al.   NATURE

Fast Resonance Assignment and Fold Determination of Human Superoxide Dismutase by High-Resolution Proton-Detected Solid-State MAS NMR Spectroscopy

(2011) Michael J. Knight et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

A Proton-Detected 4D Solid-State NMR Experiment for Protein Structure Determination

(2011) Matthias Huber et al.   CHEMPHYSCHEM

Assignment strategies for aliphatic protons in the solid-state in randomly protonated proteins

(2011) Sam Asami et al.   JOURNAL OF BIOMOLECULAR NMR

Enhanced Resolution and Coherence Lifetimes in the Solid-State NMR Spectroscopy of Perdeuterated Proteins under Ultrafast Magic-Angle Spinning

(2011) Józef R. Lewandowski et al.   Journal of Physical Chemistry Letters

Stereospecific Isotopic Labeling of Methyl Groups for NMR Spectroscopic Studies of High-Molecular-Weight Proteins

(2010) Pierre Gans et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

High Resolution1H-Detected Solid-State NMR Spectroscopy of Protein Aliphatic Resonances: Access to Tertiary Structure Information

(2010) Sam Asami et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Measurement of Site-Specific13C Spin−Lattice Relaxation in a Crystalline Protein

(2010) Józef R. Lewandowski et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Optimum levels of exchangeable protons in perdeuterated proteins for proton detection in MAS solid-state NMR spectroscopy

(2009) Ümit Akbey et al.   JOURNAL OF BIOMOLECULAR NMR

Residual methyl protonation in perdeuterated proteins for multi-dimensional correlation experiments in MAS solid-state NMR spectroscopy

(2008) Vipin Agarwal et al.   JOURNAL OF MAGNETIC RESONANCE

High-performance solvent suppression for proton detected solid-state NMR

(2008) Donghua H. Zhou et al.   JOURNAL OF MAGNETIC RESONANCE

Protein Side-Chain Dynamics As Observed by Solution- and Solid-State NMR Spectroscopy: A Similarity Revealed

(2008) Vipin Agarwal et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Amyloid Fibrils of the HET-s(218-289) Prion Form a   Solenoid with a Triangular Hydrophobic Core

(2008) C. Wasmer et al.   SCIENCE