A model for a solvent-free synthetic organic research laboratory: click-mechanosynthesis and structural characterization of thioureas without bulk solvents

Mechanochemical reactions of coordination polymers by grinding with KBr

(2012) Mangayarkarasi Nagarathinam et al.   CHEMICAL COMMUNICATIONS

Recent efforts directed to the development of more sustainable asymmetric organocatalysis

(2012) José G. Hernández et al.   CHEMICAL COMMUNICATIONS

The crystal structure of l-arginine

(2012) Emilie Courvoisier et al.   CHEMICAL COMMUNICATIONS

Supramolecular concepts and new techniques in mechanochemistry: cocrystals, cages, rotaxanes, open metal–organic frameworks

(2012) Tomislav Friščić   CHEMICAL SOCIETY REVIEWS

Desmotropy, Polymorphism, and Solid-State Proton Transfer: Four Solid Forms of an Aromatic o-Hydroxy Schiff Base

(2012) Mirta Rubčić et al.   CHEMISTRY-A EUROPEAN JOURNAL

Click Mechanochemistry: Quantitative Synthesis of “Ready to Use” Chiral Organocatalysts by Efficient Two-Fold Thiourea Coupling to Vicinal Diamines

(2012) Vjekoslav Štrukil et al.   CHEMISTRY-A EUROPEAN JOURNAL

Preparation of Chiral Amino Esters by Asymmetric Phase-Transfer Catalyzed Alkylations of Schiff Bases in a Ball Mill

(2012) Pierrick Nun et al.   CHEMISTRY-A EUROPEAN JOURNAL

Co-crystals of caffeine and piracetam with 4-hydroxybenzoic acid: Unravelling the hidden hydrates of 1 : 1 co-crystals

(2012) Srinivasulu Aitipamula et al.   CRYSTENGCOMM

Mechanochemical interconversion between discrete complexes and coordination networks – formal hydration/dehydration by LAG

(2012) Pipi Wang et al.   CRYSTENGCOMM

The role of mechanochemistry and supramolecular design in the development of pharmaceutical materials

(2012) Amit Delori et al.   CRYSTENGCOMM

Fast, solvent-free and hydrogen-bonding-mediated asymmetric Michael addition in a ball mill

(2012) Yi-Feng Wang et al.   GREEN CHEMISTRY

Mechanosynthesis of nitrosobenzenes: a proof-of-principle study in combining solvent-free synthesis with solvent-free separations

(2012) Igor Huskić et al.   GREEN CHEMISTRY

From Anion Receptors to Transporters

(2011) Philip A. Gale   ACCOUNTS OF CHEMICAL RESEARCH

A Cocrystal Strategy to Tune the Luminescent Properties of Stilbene-Type Organic Solid-State Materials

(2011) Dongpeng Yan et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Mechanosynthesis of the Metallodrug Bismuth Subsalicylate from Bi2O3 and Structure of Bismuth Salicylate without Auxiliary Organic Ligands

(2011) Vânia André et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Multinuclear solid-state NMR of square-planar platinum complexes — Cisplatin and related systems

(2011) Bryan E.G. Lucier et al.   CANADIAN JOURNAL OF CHEMISTRY

Thiourea isosteres as anion receptors and transmembrane transporters

(2011) Marco Wenzel et al.   CHEMICAL COMMUNICATIONS

Overcoming hydrolytic sensitivity and low solubility of phosphitylation reagents by combining ionic liquids with mechanochemistry

(2011) Christopher Hardacre et al.   CHEMICAL COMMUNICATIONS

Structure and magnetic ordering of a 2-D MnII(TCNE)I(OH2) (TCNE = tetracyanoethylene) organic-based magnet (Tc = 171 K)

(2011) Saul H. Lapidus et al.   CHEMICAL COMMUNICATIONS

Fast, ligand- and solvent-free copper-catalyzed click reactions in a ball mill

(2011) Rico Thorwirth et al.   CHEMICAL COMMUNICATIONS

Ball milling in organic synthesis: solutions and challenges

(2011) Achim Stolle et al.   CHEMICAL SOCIETY REVIEWS

Mechanochemistry: opportunities for new and cleaner synthesis

(2011) Stuart L. James et al.   CHEMICAL SOCIETY REVIEWS

Alternative energy input: mechanochemical, microwave and ultrasound-assisted organic synthesis

(2011) R. B. Nasir Baig et al.   CHEMICAL SOCIETY REVIEWS

Fast, Ligand- and Solvent-Free Synthesis of 1,4-Substituted Buta-1,3-diynes by Cu-Catalyzed Homocoupling of Terminal Alkynes in a Ball Mill

(2011) Robert Schmidt et al.   CHEMISTRY-A EUROPEAN JOURNAL

Effect of Fluorination on Molecular Conformation in the Solid State: Tuning the Conformation of Cocrystal Formers

(2011) Tomislav Friščić et al.   CRYSTAL GROWTH & DESIGN

Probing Intermolecular Crystal Packing in γ-Indomethacin by High-Resolution1H Solid-State NMR Spectroscopy

(2011) Jonathan P. Bradley et al.   CRYSTAL GROWTH & DESIGN

Solvent-Free Polymorphism Control in a Covalent Mechanochemical Reaction

(2011) Dominik Cinčić et al.   CRYSTAL GROWTH & DESIGN

Liquid-assisted solid-state reaction: assembly of (6,3) and (10,3) hydrogen-bonded networks based on [M(Hbiim)3] by oxidation of [M(H2biim)3]2+ complexes in the presence of acetate anions

(2011) Yu-Hui Tan et al.   CRYSTENGCOMM

Mechanosensitive metal–ligand bonds in the design of new coordination compounds

(2011) Krunoslav Užarević et al.   CRYSTENGCOMM

Hydrogen bonding interactions with the thiocarbonyl π-system

(2011) Joseph T. Lenthall et al.   CRYSTENGCOMM

A rational approach to screen for hydrated forms of the pharmaceutical derivative magnesium naproxen using liquid-assisted grinding

(2011) Tomislav Friščić et al.   CRYSTENGCOMM

Clean and rapid synthesis of double metal cyanide complexes using mechanochemistry

(2011) Wuyuan Zhang et al.   GREEN CHEMISTRY

Synthesis, Structure–Activity Relationship, and Antimalarial Activity of Ureas and Thioureas of 15-Membered Azalides

(2011) Mirjana Bukvić Krajačić et al.   JOURNAL OF MEDICINAL CHEMISTRY

Asymmetric Aldol Reaction Organocatalyzed by (S)-Proline-Containing Dipeptides: Improved Stereoinduction under Solvent-Free Conditions

(2011) José G. Hernández et al.   JOURNAL OF ORGANIC CHEMISTRY

Facile Mechanosynthesis of Amorphous Zeolitic Imidazolate Frameworks

(2011) Thomas D. Bennett et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Synthesis of Azines in Solid State: Reactivity of Solid Hydrazine with Aldehydes and Ketones

(2011) Byeongno Lee et al.   ORGANIC LETTERS

Crystal structure determination of the silver carboxylate dimer [Ag(O2C22H43)]2, silver behenate, using powder X-ray diffraction methods

(2011) Thomas N. Blanton et al.   POWDER DIFFRACTION

Solvent-free reactions of alkynes in ball mills: It is definitely more than mixing

(2011) Achim Stolle et al.   PURE AND APPLIED CHEMISTRY

Applications of high-resolution 1H solid-state NMR

(2011) Steven P. Brown   SOLID STATE NUCLEAR MAGNETIC RESONANCE

Efficient ball-mill procedure in the ‘green’ asymmetric aldol reaction organocatalyzed by (S)-proline-containing dipeptides in the presence of water

(2011) José G. Hernández et al.   TETRAHEDRON

Inclusion of aliphatic alcohols in pockets of (S)-threonyl-(S)-phenylglycine using grinding method

(2011) Motohiro Akazome et al.   TETRAHEDRON

Solvent-free synthesis of hydrazones and their subsequent N-alkylation in a Ball-mill

(2011) Pierrick Nun et al.   TETRAHEDRON

Solvent-free asymmetric aldol reaction organocatalyzed by (S)-proline-containing thiodipeptides under ball-milling conditions

(2011) José G. Hernández et al.   TETRAHEDRON

Solid-state dynamic combinatorial chemistry: reversibility and thermodynamic product selection in covalent mechanosynthesis

(2011) Ana M. Belenguer et al.   Chemical Science

1-(4-Hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)thiourea

(2010) Hyeong Choi et al.   ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE

The Crystal Structure of D-Ribose-At Last!

(2010) Dubravka Šišak et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Supramolecular Catalysis in the Organic Solid State through Dry Grinding

(2010) Anatoliy N. Sokolov et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

High Reactivity of Metal-Organic Frameworks under Grinding Conditions: Parallels with Organic Molecular Materials

(2010) Wenbing Yuan et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Rapid Room-Temperature Synthesis of Zeolitic Imidazolate Frameworks by Using Mechanochemistry

(2010) Patrick J. Beldon et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Towards an environmentally-friendly laboratory: dimensionality and reactivity in the mechanosynthesis of metal–organic compounds

(2010) Vjekoslav Štrukil et al.   CHEMICAL COMMUNICATIONS

Mechanochemistry of magnesium oxide revisited: facile derivatisation of pharmaceuticals using coordination and supramolecular chemistry

(2010) Ernest H. H. Chow et al.   CHEMICAL COMMUNICATIONS

Selective transformation pathways between crystalline forms of an organic material established from powder X-ray diffraction analysis

(2010) Kotaro Fujii et al.   CHEMICAL COMMUNICATIONS

Direct structure elucidation by powder X-ray diffraction of a metal–organic framework material prepared by solvent-free grinding

(2010) Kotaro Fujii et al.   CHEMICAL COMMUNICATIONS

A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination viaco-crystallisation

(2010) Manza B. J. Atkinson et al.   CHEMICAL COMMUNICATIONS

An Alternative Solvent-Free Synthesis of Nopinone under Ball-Milling Conditions: Investigation of Reaction Parameters

(2010) Tony Szuppa et al.   ChemSusChem

A Comparison of Cocrystal Structure Solutions from Powder and Single Crystal Techniques

(2010) Saul H. Lapidus et al.   CRYSTAL GROWTH & DESIGN

Liquid-Assisted Solid-State Reaction: Formation of a Three-Dimensional Hydrogen-Bonded Network and Evidence for Proton Induced Electron Transfer

(2010) Li-Fei Yang et al.   CRYSTAL GROWTH & DESIGN

Nitrate Ion Assisted Argentophilic Interactions as a Template for Solid State [2 + 2] Photodimerization of Pyridyl Acrylic Acid, Its Methyl Ester, and Acryl Amide

(2010) Ramkinkar Santra et al.   CRYSTAL GROWTH & DESIGN

A stepwise mechanism and the role of water in the liquid-assisted grinding synthesis of metal–organic materials

(2010) Fiona C. Strobridge et al.   CRYSTENGCOMM

Mechanochemical preparation of adducts (co-crystals and molecular salts) of 1,4-diazabicyclo-[2.2.2]-octane with aromatic polycarboxylic acids

(2010) Samipillai Marivel et al.   CRYSTENGCOMM

Mechanochemical synthesis of homo- and hetero-rare-earth(iii) metal–organic frameworks by ball milling

(2010) Wenbing Yuan et al.   CRYSTENGCOMM

Study of the mechanochemical formation and resulting properties of an archetypal MOF: Cu3(BTC)2 (BTC = 1,3,5-benzenetricarboxylate)

(2010) Wenbing Yuan et al.   CRYSTENGCOMM

Supramolecular metathesis: co-former exchange in co-crystals of pyrazine with (R,R)-, (S,S)-, (R,S)- and (S,S/R,R)-tartaric acid

(2010) Dario Braga et al.   CRYSTENGCOMM

Schiff base derived from 2-hydroxy-1-naphthaldehyde and liquid-assisted mechanochemical synthesis of its isostructural Cu(ii) and Co(ii) complexes

(2010) Dominik Cinčić et al.   CRYSTENGCOMM

Structural and spectroscopic studies of some adducts of silver(i) halides with thiourea and N-ethyl substituted thioureas

(2010) Graham A. Bowmaker et al.   DALTON TRANSACTIONS

Solvent-free dehydrogenation of γ-terpinene in a ball mill: investigation of reaction parameters

(2010) Tony Szuppa et al.   GREEN CHEMISTRY

Coordination Chemistry in the Solid State: Reactivity of Manganese and Cadmium Chlorides with Imidazole and Pyrazole and Their Hydrochlorides

(2010) Christopher J. Adams et al.   INORGANIC CHEMISTRY

(Bis)urea and (Bis)thiourea Inhibitors of Lysine-Specific Demethylase 1 as Epigenetic Modulators

(2010) Shiv K. Sharma et al.   JOURNAL OF MEDICINAL CHEMISTRY

NMR Crystallography of Campho[2,3-c]pyrazole (Z′ = 6): Combining High-Resolution1H-13C Solid-State MAS NMR Spectroscopy and GIPAW Chemical-Shift Calculations

(2010) Amy L. Webber et al.   JOURNAL OF PHYSICAL CHEMISTRY A

Thiourea as a Template for Photodimerization of Azastilbenes

(2010) Balakrishna R. Bhogala et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Powder Crystallography by Combined Crystal Structure Prediction and High-Resolution1H Solid-State NMR Spectroscopy

(2010) Elodie Salager et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Solid-state reactivity of copper(i) iodide: luminescent 2D-coordination polymers of CuI with saturated bidentate nitrogen bases

(2010) Dario Braga et al.   NEW JOURNAL OF CHEMISTRY

Oxime Decorated Cavitands Functionalized through Solvent-Assisted Grinding

(2010) Christer B. Aakeröy et al.   ORGANIC LETTERS

Mono- and bis(dialkyl/aryl dithiocarbamato) complexes of 1,1,2,3,4,5,6-heptahydro-1,1-dihalido telluranes: Synthesis, spectroscopy, structures and cleavage reaction

(2010) Prakash C. Srivastava et al.   POLYHEDRON

Detecting solid-state reactivity in 10-hydroxy-10,9-boroxophenanthrene using NMR spectroscopy

(2010) Diego Carnevale et al.   TETRAHEDRON

A simple thiourea based colorimetric sensor for cyanide anion

(2010) Maurice O. Odago et al.   TETRAHEDRON

1,3-Bis(3-methylphenyl)thiourea: triclinic polymorph

(2009) Durre Shahwar et al.   ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE

1-[2-(2,4-Dinitrobenzylideneamino)phenyl]-3-phenylthiourea

(2009) M. Umadevi et al.   ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE

Ion- and Liquid-Assisted Grinding: Improved Mechanochemical Synthesis of Metal-Organic Frameworks Reveals Salt Inclusion and Anion Templating

(2009) Tomislav Friščić et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Crystal Forms of the Antibiotic 4-Aminosalicylic Acid: Solvates and Molecular Salts with Dioxane, Morpholine, and Piperazine

(2009) Vânia André et al.   CRYSTAL GROWTH & DESIGN

Synthesis and Structural Characterization of Cocrystals and Pharmaceutical Cocrystals: Mechanochemistry vs Slow Evaporation from Solution

(2009) David R. Weyna et al.   CRYSTAL GROWTH & DESIGN

Recent Advances in Understanding the Mechanism of Cocrystal Formation via Grinding

(2009) Tomislav Friščić et al.   CRYSTAL GROWTH & DESIGN

Drug-containing coordination and hydrogen bonding networks obtained mechanochemically

(2009) Dario Braga et al.   CRYSTENGCOMM

Nonlinear effects in proline-catalysed aldol reactions under solvent-free conditions based on the ternary phase behaviour of scalemic proline

(2009) Angelika Bruckmann et al.   CRYSTENGCOMM

Mechanochemical conversion of a metal oxide into coordination polymers and porous frameworks using liquid-assisted grinding (LAG)

(2009) Tomislav Friščić et al.   CRYSTENGCOMM

The mechanochemical synthesis of podand anion receptors

(2009) Adam N. Swinburne et al.   CRYSTENGCOMM

1 : 1 complexes of silver(i) thiocyanate with (substituted) thiourea ligands

(2009) Graham A. Bowmaker et al.   DALTON TRANSACTIONS

Novel ureas and thioureas of 15-membered azalides with antibacterial activity against key respiratory pathogens

(2009) Mirjana Bukvić Krajačić et al.   EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY

Complexation Behavior of a Supramolecular Organic Fluorophore Prepared by Solid-State Co-Grinding Crystallization Using 2-Anthracenecarboxylic Acid and (R)-1-(2-Naphthyl)ethylamine and Its Optical Properties

(2009) Yoshitane Imai et al.   EUROPEAN JOURNAL OF ORGANIC CHEMISTRY

Energetic assessment of the Suzuki–Miyaura reaction: a curtate life cycle assessment as an easily understandable and applicable tool for reaction optimization

(2009) Franziska Schneider et al.   GREEN CHEMISTRY

Application of Solid-State209Bi NMR to the Structural Characterization of Bismuth-Containing Materials

(2009) Hiyam Hamaed et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Mechanically induced reactions in organic solids: liquid eutectics or solid-state processes?

(2009) Oleksandr Dolotko et al.   NEW JOURNAL OF CHEMISTRY

Third structure determination by powder diffractometry round robin (SDPDRR-3)

(2009) A. Le Bail et al.   POWDER DIFFRACTION

1-{2-[(Anthracen-10-yl)methyleneamino]phenyl}-3-phenylthiourea

(2008) D. Gayathri et al.   ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE

Anion receptor chemistry: highlights from 2007

(2008) Claudia Caltagirone et al.   CHEMICAL SOCIETY REVIEWS

Vapour Induced Crystalline Transformation Investigated byab initioPowder X-ray Diffraction Analysis

(2008) Kotaro Fujii et al.   CRYSTAL GROWTH & DESIGN

Simple and quantitative mechanochemical preparation of the first zinc and copper complexes of the neuroleptic drug gabapentin

(2008) Dario Braga et al.   CRYSTENGCOMM

The role of solvent in mechanochemical and sonochemical cocrystal formation: a solubility-based approach for predicting cocrystallisation outcome

(2008) Tomislav Friščić et al.   CRYSTENGCOMM

Control and interconversion of cocrystal stoichiometry in grinding: stepwise mechanism for the formation of a hydrogen-bonded cocrystal

(2008) Shyam Karki et al.   CRYSTENGCOMM

Synthesis and structure of two new (guanidinate)boron dichlorides and their attempted conversion to boron(i) derivatives

(2008) Michael Findlater et al.   DALTON TRANSACTIONS

Unexpected Solvent-Free Cycloadditions of 1,3-Cyclohexanediones to 1-(Pyridin-2-yl)-enones Mediated by Manganese(III) Acetate in a Ball Mill

(2008) Guan-Wu Wang et al.   JOURNAL OF ORGANIC CHEMISTRY

Application of Solid-State35Cl NMR to the Structural Characterization of Hydrochloride Pharmaceuticals and their Polymorphs

(2008) Hiyam Hamaed et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Novel Bifunctional Chiral Thiourea Catalyzed Highly Enantioselective aza-Henry Reaction†

(2008) Chungui Wang et al.   ORGANIC LETTERS

Thiourea-catalyzed Morita–Baylis–Hillman reaction

(2008) Yoshihiro Sohtome et al.   TETRAHEDRON

Isostructural Materials Achieved by Using Structurally Equivalent Donors and Acceptors in Halogen-Bonded Cocrystals

(2007) Dominik Cinčić et al.   CHEMISTRY-A EUROPEAN JOURNAL

Synthesis of some novel thiourea derivatives obtained from 5-[(4-aminophenoxy)methyl]-4-alkyl/aryl-2,4-dihydro-3H-1,2,4-triazole-3-thiones and evaluation as antiviral/anti-HIV and anti-tuberculosis agents

(2007) İlkay Küçükgüzel et al.   EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY