Journal
CHEMSUSCHEM
Volume 8, Issue 3, Pages 443-447Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cssc.201402827
Keywords
aniline; carbamate; carbon recycling; methyl formate; oxidative carbonylation
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Methyl N-phenyl carbamate was synthesized from aniline by using methyl formate as a green and efficient carbonylating agent. High yields were obtained at milder reaction conditions compared to the conventional CO/CH3OH route. Studies on the reaction sequence led to suggest an alternative and more efficient route to the carbamate via formanilide as intermediate.
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