Article
Chemistry, Analytical
Nur Cebi, Ozun Gorel Manav, Elmas Oktem Olgun
Summary: This research developed an analytical methodology to efficiently monitor 77 pesticides in hazelnut samples, validated the method's effectiveness, and successfully applied it to real hazelnut samples. Various pesticide residues were detected in commercial hazelnuts, but the quantities were significantly lower than the maximum residue limits published by the European Union.
MICROCHEMICAL JOURNAL
(2021)
Article
Food Science & Technology
Hyungju Seo, Sunyeong Jang, Hyeongwook Jo, Haejin Kim, Seunghwa Lee, Hyejeong Yun, Minhee Jeong, Joonkwan Moon, Taewoong Na, Hyunjeong Cho
Summary: The study optimized the QuEChERS-based method for the analysis of 11 mycotoxins in feed samples, revealing occurrence rates of FBs, ZEN, and DON at 59.4%, 38.0%, and 32.1%, respectively. Co-occurrence of two or three mycotoxins in feed samples was common, emphasizing the need for stricter management standards for FBs, DON, and ZEN in South Korea.
Article
Chemistry, Analytical
Nermine Fares, Yasmeen A. A. Hassan, Lobna A. Hussein, Miriam F. Ayad
Summary: A new LC-MS/MS method was successfully developed for the determination of five fungicides in orange samples, with optimized parameters for accurate quantification below maximum residue limits. This method was applied to quantify residues in market and organic orange samples, and also to study the degradation kinetics and half-lives of these fungicides in citrus fruits for the first time.
MICROCHEMICAL JOURNAL
(2021)
Article
Environmental Sciences
Isra Toptanci, Mustafa Kiralan, Mohamed Fawzy Ramadan
Summary: In this study, pesticide residues in 493 fruit and vegetable samples from markets in Turkey were detected using a highly efficient extraction method. The results showed that nearly half of the samples were contaminated, with 30% of them containing pesticide residues above maximum residue limits. Chlorpyrifos was the most commonly detected pesticide, affecting a variety of different crops.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2021)
Article
Agriculture, Multidisciplinary
Feride Oyku Sefiloglu, Ulas Tezel, Isil Akmehmet Balcioglu
Summary: The contamination of agricultural soil and crops is a global issue. In this study, a QuEChERS extraction coupled with LC-MS/MS quantification method was used for the first time to measure 65 emerging contaminants in soil and rice. Various pesticides and industrial chemicals were detected in soil, with pesticide residues present in all soil samples and industrial pollutants found in paddy soil samples. However, the concentrations of these contaminants in rice were below their maximum residual limits.
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
(2021)
Article
Chemistry, Applied
R. Harischandra Naik, M. S. Pallavi, Nandini, A. Shwetha, M. Bheemanna, R. Udaykumar Nidoni
Summary: An LC-MS/MS method was developed and validated for analyzing pesticides in pomegranate whole fruits and arils. The method demonstrated high accuracy and reproducibility, and can detect and quantify a wide range of pesticides in pomegranate samples.
Article
Food Science & Technology
Jelena Radulovic, Milica Lucic, Aleksandra Nesic, Antonije Onjia
Summary: This study investigated the occurrence of pesticide residues on citrus fruits and evaluated the acute and chronic risk for adults and children. Multiple residues were detected in 83% of the samples analyzed, and 28% contained pesticides at or above maximum residue levels. Most detected pesticides posed a low risk, but some exceeded the acceptable levels for acute and chronic dietary risk. The acute risk was unacceptable in 5.3% of citrus fruits for adults and 26% for children.
Article
Plant Sciences
Kun Zhang, Jing Ma, Sunil S. Gangurde, Lei Hou, Han Xia, Nana Li, Jiaowen Pan, Ruizheng Tian, Huailing Huang, Xingjun Wang, Yindong Zhang, Chuanzhi Zhao
Summary: In this study, metabolite profiling was performed on four peanut germplasm lines with different testa colors. A total of 85 metabolites were identified, and 78 differentially accumulated metabolites were found. The results showed significant differences in the accumulation of metabolites in testa with different colors, providing valuable information for further investigation of biosynthesis and accumulation mechanisms of these metabolites in peanut.
FRONTIERS IN PLANT SCIENCE
(2022)
Article
Chemistry, Analytical
Sudip Bhattacharyya, Rajlakshmi Poi, Moni Baskey Sen, Dipak Kumar Hazra, Rajarshi Ghosh, Swagata Mandal, Rajib Karmakar
Summary: This study developed a modified QuEChERS method for the quick and accurate screening of multi-class multi-pesticide residues in betelvine. 9% of the collected market samples were found to be contaminated with non-recommended pesticides, but the human risk indexes were within the acceptable range.
MICROCHEMICAL JOURNAL
(2022)
Article
Environmental Sciences
Syeda Nazish Ali, Nazia Rafique, Shazia Akhtar, Touqeer Taj, Farrakh Mehboob
Summary: The EURL-FV-2010-M1 method was used to determine pesticide residues in okra, and it was found that 62% of the tested samples were contaminated, with three samples exceeding the EU maximum residue limits. The estimated daily intake of the detected pesticides was within a safe range, and there were insignificant risks from chronic exposure and minor to medium risks from acute exposure to human health.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2022)
Article
Food Science & Technology
Georgiana-Diana Dumitriu Gabur, Iulian Gabur, Elena Iulia Cucolea, Teodor Costache, Dan Rambu, Valeriu V. Cotea, Carmen Teodosiu
Summary: This study analyzed the pesticide residues in wines and found that the concentrations of pesticide residues in these samples do not pose any immediate risk to consumers. However, pesticide residue intake has been associated with health problems, making it crucial to monitor their presence in horticultural crops for clean and safe food products and healthy consumers.
Article
Chemistry, Applied
Ozgur Golge, Seren Cinpolat, Bulent Kabak
Summary: The study assessed the occurrence and quantification of pesticides in gherkins cultivated in Turkey, finding that a proportion of samples contained pesticide residues, some of which were not approved in the EU. Multiple pesticide residues were detected in some samples, with some exceeding the maximum residue levels.
JOURNAL OF FOOD COMPOSITION AND ANALYSIS
(2021)
Article
Environmental Sciences
Andrea Acosta-Dacal, Cristian Rial-Berriel, Ricardo Diaz-Diaz, Maria del Mar Bernal-Suarez, Octavio P. Luzardo
Summary: The modified QuEChERS method optimized for the extraction of 218 pesticide residues in agricultural soil samples showed high accuracy and sensitivity when applied to actual samples. The method demonstrated excellent performance in terms of quantification and detection limits.
SCIENCE OF THE TOTAL ENVIRONMENT
(2021)
Article
Environmental Sciences
Carolin Friedle, Klaus Wallner, Peter Rosenkranz, Dieter Martens, Walter Vetter
Summary: Research conducted in a fruit-growing area in Southern Germany found that almost 90% of daily pollen samples analyzed featured between one and thirteen different pesticides, with maximum concentrations reaching up to 4500 ng/g. Maximum residual concentrations of pesticides were observed mainly in April, the first half of May, and the second half of June. Data showed a pattern of pesticide residuals peaking for approximately 10 subsequent days with two or three maximum values.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2021)
Article
Environmental Sciences
Fatma Hepsag, Tefide Kizildeniz
Summary: This research assessed the health risks associated with pesticide residues in greenhouse grown tomato production in the Mediterranean Region of Turkey. The study found that most samples contained pesticide residues and exceeded the maximum residue levels permitted by the EU guidelines.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2021)