Journal
NANOMATERIALS
Volume 10, Issue 3, Pages -Publisher
MDPI
DOI: 10.3390/nano10030580
Keywords
cobalt ferrite; metal doping; sol-gel; nanocomposites; magnetic properties
Categories
Funding
- Romanian Research and Innovation Ministry [19PFE/2018 PROINSTITUTIO]
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This paper presents the synthesis of metal doped Co ferrites, M0.2Co0.8Fe2O4 (M = Cu2+, Ni2+, and Zn2+) embedded in SiO2 matrix by an innovative sol-gel route. The structural and morphological characterization provided information about the crystalline phases, crystallite size, and the shape of the prepared ferrites. The thermal study depicted the thermal decomposition and stability of the obtained ferrites. X-ray diffraction indicated nanocrystalline ferrites with spinel structure and the lack of crystalline phase impurities, while Fourier transform infrared spectroscopy revealed the presence of functional groups in precursors and ferrite powders. The lattice parameters showed a gradual increase indicating a uniform distribution of divalent metal ions in the Co ferrite lattice. The crystallite size, magnetic moment, super-exchange and deflection of magnetic domain were influenced by the dopant metal ion. The room temperature magnetization indicated a ferromagnetic behavior of the ferrites annealed at 1000 degrees C and a superparamagnetic behavior of the ferrites annealed at 700 degrees C.
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