Journal
FOOD CHEMISTRY
Volume 294, Issue -, Pages 160-170Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2019.05.022
Keywords
Bisphenol compounds; Chemometrics; Daily dietary exposure; Foodstuffs; QuEChERS; Solid-phase extraction
Funding
- Public Welfare Technology Research Program/Analysis and Testing Project of Zhejiang Natural Fund [LGC19H260002]
- National Natural Science Foundation of China [21677128]
- Zhejiang Provincial Natural Science Foundation of China [LY18B050001]
- Medical and Health Science and Technology Plan of Zhejiang Province [2018266692, 2018258376, 2018270577]
- Ningbo science and technology innovation team [2015C110019]
- Ningbo Health Branding Subject Fund [ppxk201810]
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An effective method has been developed for the simultaneous determination of four bisphenols (bisphenol A, S, F and B) in various foodstuffs. The contaminants were extracted by QuEChERS-based strategy and subjected to ion-exchange solid-phase extraction for further clean-up. The critical variables were screened by Plackett-Burman design and then optimized by central composite design. Under the optimized conditions, satisfactory accuracy (recoveries 76%-116%) and precision (RSDs < 12%) were achieved. The established method was then used to assess the contamination status of 379 real samples. Bisphenol A was demonstrated to be the predominant bisphenol with highest incidence (79.7%) and average concentration (14.3 mu g/kg). The positive rates (mean concentration) of bisphenol S, F and B were 37.7% (1.6 mu g/kg), 26.9% (1.4 mu g/kg) and 0.0% (not detected), respectively. Finally, the daily dietary intakes of Sigma(4) bisphenolsfor adult residents were estimated (55.9-76.1 ng/kg bw/day) according to the contamination concentrations and the daily recommended intakes.
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