Journal
ACS OMEGA
Volume 4, Issue 9, Pages 14085-14091Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acsomega.9b01951
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Funding
- Russian Science Foundation [18-73-10030]
- Russian Science Foundation [18-73-10030] Funding Source: Russian Science Foundation
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The first total synthesis of natural acetogenin, chatenaytrienin-1, was performed in 10 steps and in 41% overall yield using cross-cyclomagnesiation of (6Z)-heptadeca-1,2,6-triene and trideca-11,12-dien-1-ol tetrahydropyran acetal with EtMgBr in the presence of Mg metal and the Cp2TiCl2 catalyst (10 mol %) as the key step of the synthesis.
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