Journal
NANOMATERIALS
Volume 9, Issue 10, Pages -Publisher
MDPI
DOI: 10.3390/nano9101349
Keywords
mono-6-deoxy-6-aminopropylamino-beta-cyclodextrin; pr-beta-CD; flavonoid; selectivity; Ag-embedded SiO2; SERS
Categories
Funding
- National Research Foundation (NRF) of Korea
- Korean Government [NRF-2017H1A2A1044051]
- WTU joint research grant of Konkuk University in 2017 [2017-A019-0334]
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It has been increasingly important to develop a highly sensitive and selective technique that is easy to handle in detecting levels of beneficial or hazardous analytes in trace quantity. In this study, mono-6-deoxy-6-aminopropylamino-beta-cyclodextrin (pr-beta-CD)-functionalized silver-assembled silica nanoparticles (SiO2@Ag@pr-beta-CD) for flavonoid detection were successfully prepared. The presence of pr-beta-CD on the surface of SiO2@Ag enhanced the selectivity in capturing quercetin and myricetin among other similar materials (naringenin and apigenin). In addition, SiO2@Ag@pr-beta-CD was able to detect quercetin corresponding to a limit of detection (LOD) as low as 0.55 ppm. The relationship between the Raman intensity of SiO2@Ag@pr-beta-CD and the logarithm of the Que concentration obeyed linearity in the range 3.4-33.8 ppm (R-2 = 0.997). The results indicate that SiO2@Ag@pr-beta-CD is a promising material for immediately analyzing samples that demand high sensitivity and selectivity of detection.
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