4.7 Article

Effect of extrusion parameters on microstructure, texture and mechanical properties of Mg-1.38Zn-0.17Y-0.12Ca (at. %) alloy

Journal

MATERIALS CHARACTERIZATION
Volume 151, Issue -, Pages 137-145

Publisher

ELSEVIER SCIENCE INC
DOI: 10.1016/j.matchar.2019.03.004

Keywords

Magnesium alloys; Dynamic recrystallization; Microstructure; Precipitation; Mechanical properties

Funding

  1. National Natural Science Foundation of China [51771129, 51401144, 51771128]
  2. Natural Science Foundation of Shanxi Province [2015021067, 201601D011034]
  3. Projects of International Cooperation in Shanxi [201703D421039]

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In this study, the effect of extrusion conditions on the microstructures, texture and tensile properties of Mg-1.38Zn-0.17Y-0.12Ca (at. %) alloys was investigated by conducting direct extrusion at different temperatures (190, 230 and 270 degrees C) and extrusion speeds (0.1 and 0.01 mm s(-1)). The results showed that grains of as-extruded Mg-1.38Zn-0.17Y-0.12Ca alloy were much finer than that of the as-cast one, which indicated that the micro structural evolution during extrusion was governed by dynamic recrystallization. The average size and volume fraction of dynamic recrystallized grains decreased with the decrease of extrusion speed or extrusion temperature. Both the average size and volume fraction of precipitated nano-sized I-phase decreased with decreasing extrusion temperature. With decreasing the extrusion speed, the average size of nano-sized I-phase decreased while the volume fraction increased. The alloy extruded at 190 degrees C and speed of 0.1 mm s(-1) showed the ultimate tensile strength of 357.0 MPa, tensile yield strength of 317.2 MPa and elongation to failure of 6.4%. The texture intensity for the as-extruded Mg-1.38Zn-0.17Y-0.12Ca alloy increased with the decrease of the extrusion speed, while the change in the texture intensity was not obvious as extrusion temperature decreased. The significantly refined grains and large amounts of nano-sized I-phase led to a higher working hardening rate. The working hardening rate curve of the alloy extruded at 270 degrees C exhibited a positive slope of strain hardening rate due to the relatively coarse grain size.

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