Journal
RSC ADVANCES
Volume 3, Issue 10, Pages 3399-3406Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ra22639a
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Funding
- Platform Chemical Process Technology from Lignocellulosic Biomass Conversion RD Program [10035574]
- Ministry of Knowledge Economy
- Ministry of Education, Science and Technology [2012-0006693]
- Priority Research Centers Program through the National Research Foundation of Korea (NRF)
- National Research Foundation of Korea [2009-0093816] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Ionic liquid (1,1'-hexane-1,6-diylbis (3-methylpyridinium) tetrachloronickelate (II)) and PVDF-IL ([C-6(mpy)(2)][NiCl4](2-)) nanofiber composites are synthesized and used as catalysts for the reduction of nitroarenes with NaBH4/H2O system at ambient temperature. Ionic liquid containing nickel halide anion well dispersed on the PVDF nanofibers. It efficiently catalyzes the reduction of functionalized nitroarenes to the corresponding substituted anilines, avoiding the need for inert atmosphere, and additional base or other additives. The catalytic system gives good yields with other functional groups remaining intact.
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