Journal
TETRAHEDRON LETTERS
Volume 55, Issue 27, Pages 3701-3705Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2014.05.010
Keywords
Suzuki-Miyaura; Cross-coupling; Ligand free catalysis; Supported palladium; Flow chemistry; Scalable process
Categories
Funding
- Fundacion Universidad-Empresa (FUE)
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An environmentally friendly continuous-flow protocol for the Suzuki coupling of boronic acids and aryl halides under ligand-free conditions using solid-supported Pd is presented. The process described herein uses very simple reaction conditions and equipment setup and can be readily scaled up to provide multigram quantities of products containing low levels of residual Pd. (C) 2014 Elsevier Ltd. All rights reserved.
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