Journal
RSC ADVANCES
Volume 5, Issue 49, Pages 38846-38850Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra05987a
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Funding
- UGC, New Delhi
- CSIR, New Delhi
- University Grant Commission, New Delhi [F.20-40(12)/2013(BSR)]
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A simple and highly efficient synthetic approach to enantiopure 2-alkyl substituted tetrahydroquinoline 1 skeleton from aldehydes as starting materials and its application to the total synthesis of (+)-angustureine 2 is described. Key transformations include proline catalyzed aminoxylation, Corey-Fuchs protocol, Sonogashira coupling and intramolecular Mitsunobu reactions.
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