Journal
RSC ADVANCES
Volume 5, Issue 65, Pages 52588-52594Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra06474k
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Funding
- Zhejiang Provincial Natural Science Foundation of China [LZ13B020001]
- National Natural Science Foundation of China [21376058]
- Major scientific and technological innovation projects of Hangzhou City [20122511A43]
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A highly efficient and practical procedure to direct ortho-sulfonylation of azobenzenes' C-H bond with arylsulfonyl chlorides has been developed. The method was applicable to both electron-rich and electron-deficient substrates and delivered good yields for 21 examples. This reaction provides a convenient access to ortho-sulfonylated azobenzenes under mild conditions.
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