4.7 Article

Evolution of intragranular stresses and dislocation densities during cyclic deformation of polycrystalline copper

Journal

ACTA MATERIALIA
Volume 94, Issue -, Pages 193-204

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.actamat.2015.04.031

Keywords

Fatigue deformation; Geometrically necessary dislocations (GNDs); Intragranular stress; High resolution electron backscattering diffraction (HR-EBSD)

Ask authors/readers for more resources

We have used the cross-correlation based high resolution electron backscattering diffraction (HR-EBSD) technique to evaluate at high spatial resolution the spatial patterning of the type III intragranular residual stresses and geometrically necessary dislocation (GND) density within polycrystalline Cu after cyclic deformation. Oxygen free high conductivity (OFHC) polycrystalline copper samples were cyclically deformed under stress-control at a load ratio of 0.1 and EBSD measurements were made at points throughout the early stages of fatigue when strain amplitudes and cyclic creep rates are changing most significantly, namely at 0 cycles, 2 cycles, 200 cycles and 2000 cycles. Statistical analysis is presented showing that moderate correlations exist between stored GND density, residual intragranular stress and distance from the nearest grain boundaries and/or triple junctions. (C) 2015 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Authors

I am an author on this paper
Click your name to claim this paper and add it to your profile.

Reviews

Primary Rating

4.7
Not enough ratings

Secondary Ratings

Novelty
-
Significance
-
Scientific rigor
-
Rate this paper

Recommended

Article Engineering, Mechanical

Bayesian optimized collection strategies for fatigue strength testing

Christopher Massimo Magazzeni, Rory Rose, Chris Gearhart, Jicheng Gong, Angus J. Wilkinson

Summary: This article presents a statistical framework for optimal sampling and analysis of constant life fatigue data. Protocols are built based on Bayesian maximum entropy sampling, reducing the need for prior knowledge in data collection. Experimental validation demonstrates the applicability of these methods in laboratory testing and shows improvements in parameter estimation efficiency and accuracy.

FATIGUE & FRACTURE OF ENGINEERING MATERIALS & STRUCTURES (2023)

Article Engineering, Environmental

Synergistic optimizing thermoelectric performance of SnTe by the integrated Multi-strategy

Xuemei Wang, Gang Wu, RuoYu Wang, Liang Xu, Haoyang Hu, Peng Sun, Xiaojian Tan, Guoqiang Liu, Jun Jiang

Summary: This study applied an integrated multistrategy, including band convergence, defect engineering, and carrier manipulation, to optimize the thermoelectric properties of SnTe. Cd-doping, Cu2Se nano-precipitate, and Sb-doping were introduced step by step to achieve the goals. The obtained compound (Sn0.86Cd0.04Sb0.1Te)0.96(Cu2Se)0.04 exhibited a high peak ZT of 1.52 at 833 K and a low thermal conductivity of 1.3 W m-1 K-1.

CHEMICAL ENGINEERING JOURNAL (2023)

Article Chemistry, Physical

Controlling microstructure and mechanical properties of Ti-V-Cr-Nb-Ta refractory high entropy alloys through heat treatments

Junliang Liu, Robert J. Scales, Bo-Shiuan Li, Michael Goode, Bradley A. Young, Jianan Hu, Angus J. Wilkinson, David E. J. Armstrong

Summary: In this study, the microstructure and mechanical properties of two refractory high entropy alloys (RHEAs) were investigated. The alloys showed similar single-phase BCC structures in different conditions, and secondary phases with different sizes and volume fractions were formed after homogenisation heat treatment. The major secondary phase was identified as a complex C15 Laves structure. The hardness of the alloys was improved after homogenisation heat treatment, and the correlations between hardness changes and microstructural evolutions were discussed.

JOURNAL OF ALLOYS AND COMPOUNDS (2023)

Article Materials Science, Multidisciplinary

HR-EBSD analysis of in situ stable crack growth at the micron scale

Abdalrhaman Koko, Thorsten H. Becker, Elsiddig Elmukashfi, Nicola M. Pugno, Angus J. Wilkinson, James Marrow

Summary: Understanding the local fracture resistance of microstructural features is crucial for the microstructure-informed design of materials. This study presents a novel approach to evaluate stress intensity factors directly from experimental measurements, using high-resolution electron backscatter diffraction. An exemplar study is conducted on a quasi-static crack propagating on low index {hkl} planes in a (001) single crystal silicon wafer.

JOURNAL OF THE MECHANICS AND PHYSICS OF SOLIDS (2023)

Article Thermodynamics

Interfacial thermal stresses of segmented thermoelectric generators

Zipeng Yan, Longbing Yi, Haowei Xu, Shaolin Huang, Kun Song, Chunrong Pan, Jun Jiang

Summary: The mechanical performance of a segmented thermoelectric generator (TEG) is investigated using theoretical and numerical methods. The results show that the structural stress depends on the ratio of cross-sectional areas between p- and n-type TE legs, while the height ratio of different segments has a significant influence on structural stress. Thermal stress induced by unmatched thermal expansion between different segments increases rapidly with the increase of cross-sectional area and can easily exceed 20% of the total interfacial stress. The conversion efficiency and interfacial stress can be optimized by adjusting the ratio of cross-sectional areas. These findings provide a theoretical basis and guidance in the design of segmented TEGs.

JOURNAL OF THERMAL STRESSES (2023)

Article Materials Science, Multidisciplinary

Transmission Kikuchi Diffraction Mapping Induces Structural Damage in Atom Probe Specimens

Baptiste Gault, Heena Khanchandani, Thoudden Sukumar Prithiv, Stoichko Antonov, T. Ben Britton

Summary: Measuring local chemistry of specific crystallographic features by atom probe tomography (APT) is aided by transmission Kikuchi diffraction (TKD), but the potential structural damage caused by TKD is often ignored. Two case studies demonstrate damage in APT specimens from TKD mapping. The damage includes planar segregation of solutes and the formation of voids containing high concentrations of a specific element.

MICROSCOPY AND MICROANALYSIS (2023)

Article Microscopy

An iterative method for reference pattern selection in high-resolution electron backscatter diffraction (HR-EBSD)

Abdalrhaman Koko, Vivian Tong, Angus J. Wilkinson, T. James Marrow

Summary: In high-resolution electron backscatter diffraction (HR-EBSD), the choice of a reference diffraction pattern (EBSP0) has a significant impact on the precision of strain and rotation mapping. This effect was observed in plastically deformed body-centered cubic and face-centered cubic ductile metals, as well as in brittle single-crystal silicon, indicating that it is not limited to measurement magnitude but also extends to spatial distribution. An empirical relationship between the cross-correlation parameter and angular error was established and utilized in an iterative algorithm to identify the optimal reference pattern for maximizing HR-EBSD precision.

ULTRAMICROSCOPY (2023)

Article Materials Science, Multidisciplinary

Efficient and Stable Gd3Ga5O12:Cr3+ Phosphors for High-Performance NIR LEDs

Chen Jin, Ruiyang Li, Yongfu Liu, Liangliang Zhang, Jiahua Zhang, Peng Sun, Zhaohua Luo, Jun Jiang

Summary: An easy strategy is reported to improve the luminescent properties of GGG:Cr3+ phosphor by optimizing the synthesized technology. The EQE is enhanced to 43.6% and the fabricated pc-LEDs achieve a high WPE of 34.3%. These results demonstrate significant advancements in NIR phosphor materials and NIR pc-LED devices.

ADVANCED OPTICAL MATERIALS (2023)

Article Engineering, Chemical

Thermoelectric Generator Design and Characterization for Industrial Pipe Waste Heat Recovery

Di Xiao, Peng Sun, Jianlin Wu, Yin Zhang, Jiehua Wu, Guoqiang Liu, Haoyang Hu, Jun Hu, Xiaojian Tan, Shi He, Jun Jiang

Summary: Thermoelectric technology is an effective strategy to convert low-grade waste heat to electrical energy directly. However, there is limited research on thermoelectric generators (TEGs) for use in industrial pipelines. In this study, an arch bridge-shaped heat collector was proposed for the pipe to recover wasted thermal energy. The effects of key factors on generating performance were studied, and the experimental results showed the feasibility of using TEGs to recover waste heat from pipes.

PROCESSES (2023)

Article Materials Science, Multidisciplinary

Calibration and data-analysis routines for nanoindentation with spherical tips

Diana Avadanii, Anna Kareer, Lars Hansen, Angus Wilkinson

Summary: Instrumented spherical nanoindentation is increasingly popular in microphysical investigations. This study tests and integrates strategies for tip and machine-stiffness calibration for spherical tips. A routine for independently calibrating effective tip radius and machine stiffness is proposed, and its validity is confirmed through benchmarks and application to different materials. The impact of machine stiffness on yield stress identification methods is also evaluated.

JOURNAL OF MATERIALS RESEARCH (2023)

Article Materials Science, Multidisciplinary

High-performance Gd3Al4GaO12:Cr3+phosphors for next-generation far-red LEDs

Chen Jin, Ruiyang Li, Yongfu Liu, Chunhui Zhou, Peng Sun, Zhaohua Luo, Zehua Liu, Jun Jiang

Summary: An excellent FR phosphor, Gd3Al4GaO12:Cr3+, with good external quantum efficiency (EQE), suitable photoluminescence, and high thermal stability is developed by optimizing the sintering technology and chemical design. The phosphor has an emission peak at 734 nm and a band width of 70 nm, matching well with the PFR absorption band. By adjusting the flux of H3BO3 and Cr3+ concentration, the EQE reaches 47.2%, and the thermal stability remains at 96.8% at 423 K. The power-conversion efficiency of the FR pc-LED reaches 24.0% driven at 100 mA, demonstrating its high performance and promising applications in the next-generation FR light source.

MATERIALS RESEARCH BULLETIN (2023)

Article Engineering, Manufacturing

Investigation of variability in apparent values of materials properties in thermo-mechanical uniaxial tensile tests on sheet metals

Ruiqiang Zhang, Jun Jiang, Jianguo Lin, Victoria A. Yardley

Summary: Thermo-mechanical uniaxial tensile testing is commonly used to characterize material properties under advanced industrial forming processes. This study investigates the effect of nonuniform temperature distributions on the variability of thermo-mechanical properties and microstructures of tested specimens.

JOURNAL OF MANUFACTURING PROCESSES (2023)

Article Geochemistry & Geophysics

The Role of Grain Boundaries in Low-Temperature Plasticity of Olivine Revealed by Nanoindentation

Diana Avadanii, Lars Hansen, Katharina Marquardt, David Wallis, Markus Ohl, Angus Wilkinson

Summary: The distribution of grain-boundary types in olivine-rich rocks might affect the mechanical behavior during deformation.

JOURNAL OF GEOPHYSICAL RESEARCH-SOLID EARTH (2023)

Article Metallurgy & Metallurgical Engineering

Achieving high ductility and strength in magnesium alloy through cryogenic-hot forming

Kai Zhang, Zhutao Shao, Joseph Robson, Yan Huang, Jinghua Zheng, Jun Jiang

Summary: A new cryogenic-hot forming process concept is proposed and proven to improve the ductility and fracture strength of magnesium alloys. This is achieved through effective grain refinement and texture weakening, making it a potential innovative method for producing high-performance magnesium components.

JOURNAL OF MAGNESIUM AND ALLOYS (2023)

Article Materials Science, Multidisciplinary

Mismatched atomic bonds and ultralow thermal conductivity in Ag-based ternary chalcopyrites

Ruoyu Wang, Jianfeng Cai, Qiang Zhang, Xiaojian Tan, Jiehua Wu, Guoqiang Liu, Jun Jiang

Summary: Diamond like ternary chalcopyrites MBX2 (M = Cu, Ag; B = Ga, In, Tl; X = S, Se, Te) have attracted significant research attention in the field of thermoelectrics due to their competitive performance and diverse transport properties. The ultralow thermal conductivity of AgBX2 compared to CuBX2 is explained by the mismatched atomic bonds between Ag-X and B -X pairs, resulting from the weaker bonding strength of Ag-X due to the expanded 4d orbital of Ag. This study provides important insights into the ultralow thermal conductivity of Ag-based ternary chalcopyrites and suggests a general strategy to suppress thermal conductivity in ternary compounds.

PHYSICAL REVIEW B (2023)

Article Materials Science, Multidisciplinary

Transmission electron microscopy of the rapid solidification microstructure evolution and solidification interface velocity determination in hypereutectic Al-20at.%Cu after laser melting

Y. Liu, K. Zweiacker, C. Liu, J. T. McKeown, J. M. K. Wiezorek

Summary: The evolution of rapid solidification microstructure and solidification interface velocity of hypereutectic Al-20at.%Cu alloy after laser melting has been studied experimentally. It was found that the formation of microstructure was dominated by eutectic, alpha-cell, and banded morphology grains, and the growth modes changed with increasing interface velocity.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Mechanisms for high creep resistance in alumina forming austenitic (AFA) alloys

Bharat Gwalani, Julian Escobar, Miao Song, Jonova Thomas, Joshua Silverstein, Andrew Chihpin Chuang, Dileep Singh, Michael P. Brady, Yukinori Yamamoto, Thomas R. Watkins, Arun Devaraj

Summary: Castable alumina forming austenitic alloys exhibit superior creep life and oxidation resistance at high temperatures. This study reveals the mechanism behind the enhanced creep performance of these alloys by suppressing primary carbide formation and offers a promising alloy design strategy for high-temperature applications.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Achieving atomically flat copper surface: Formation of mono-atomic steps and associated strain energy mechanisms

Jian Song, Qi Zhang, Songsong Yao, Kunming Yang, Houyu Ma, Jiamiao Ni, Boan Zhong, Yue Liu, Jian Wang, Tongxiang Fan

Summary: Recent studies have shown that achieving an atomically flat surface for metals can greatly improve their oxidation resistance and enhance their electronic-optical applications. Researchers have explored the use of graphene as a covering layer to achieve atomically flat surfaces. They found that high-temperature deposited graphene on copper surfaces formed mono-atomic steps, while annealed copper and transferred graphene on copper interfaces formed multi-atomic steps.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Modeling and measurements of creep deformation in laser-melted Al-Ti-Zr alloys with bimodal grain size

Jennifer A. Glerum, Jon-Erik Mogonye, David C. Dunand

Summary: Elemental powders of Al, Ti, Sc, and Zr are blended and processed via laser powder-bed fusion to create binary and ternary alloys. The microstructural analysis and mechanical testing show that the addition of Ti results in the formation of primary precipitates, while the addition of Sc and Zr leads to the formation of fine grain bands. The Al-0.25Ti-0.25Zr alloy exhibits comparable strain rates to Al-0.5Zr at low stresses, but significantly higher strain rates at higher stresses during compressive creep testing. Finite element modeling suggests that the connectivity of coarse and fine grain regions is a critical factor affecting the creep resistance of the alloys.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Characterizing stable nanocrystalline Cu-Ta behavior and failure dynamics under extremes of strain rate, strain, temperature and pressure by modified dynamic tensile extrusion

P. Jannotti, B. C. Hornbuckle, J. T. Lloyd, N. Lorenzo, M. Aniska, T. L. Luckenbaugh, A. J. Roberts, A. Giri, K. A. Darling

Summary: This work characterizes the thermo-mechanical behavior of bulk nanocrystalline Cu-Ta alloys under extreme conditions. The experiments reveal that the alloys exhibit unique mechanical properties, behaving differently from conventional nanocrystalline Cu. They do not undergo grain coarsening during extrusion and exhibit behavior similar to coarse-grained Cu.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Phase-dependent microstructure modification leads to high thermoelectric performance in n-type layered SnSe2

Yiqing Wei, Jingwei Li, Daliang Zhang, Bin Zhang, Zizhen Zhou, Guang Han, Guoyu Wang, Carmelo Prestipino, Pierric Lemoine, Emmanuel Guilmeau, Xu Lu, Xiaoyuan Zhou

Summary: This study proposes a new strategy to modify microstructure by phase regulation, which can simultaneously enhance carrier mobility and reduce lattice thermal conductivity. The addition of Cu in layered SnSe2 induces a phase transition that leads to increased grain size and reduced stacking fault density, resulting in improved carrier mobility and lower lattice thermal conductivity.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Selective oxidation and nickel enrichment hinders the repassivation kinetics of multi-principal element alloy surfaces

Jia Chen, Zhengyu Zhang, Eitan Hershkovitz, Jonathan Poplawsky, Raja Shekar Bhupal Dandu, Chang-Yu Hung, Wenbo Wang, Yi Yao, Lin Li, Hongliang Xin, Honggyu Kim, Wenjun Cai

Summary: In this study, the structural origin of the pH-dependent repassivation mechanisms in multi-principal element alloys (MPEA) was investigated using surface characterization and computational simulations. It was found that selective oxidation in acidic to neutral solutions leads to enhanced nickel enrichment on the surface, resulting in reduced repassivation capability and corrosion resistance.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Rate-dependent transition of dislocation mechanisms in a magnesium alloy

X. Y. Xu, C. P. Huang, H. Y. Wang, Y. Z. Li, M. X. Huang

Summary: The limited slip systems of magnesium (Mg) and its alloys hinder their wide applications. By conducting tensile straining experiments, researchers discovered a rate-dependent transition in the dislocation mechanisms of Mg alloys. At high strain rates, glissile dislocations dominate, while easy-glide dislocations dominate at low strain rates. Abundant glissile dislocations do not necessarily improve ductility.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

The effect of temperature on detwinning and mechanical properties of face-centered cubic deformation twins

M. S. Szczerba, M. J. Szczerba

Summary: Inverse temperature dependences of the detwinning stress were observed in face-centered cubic deformation twins in Cu-8at.%Al alloy. The detwinning stress increased with temperature when the pi detwinning mode was involved, but decreased when the pi/3 mode was involved. The dual effect of temperature on the detwinning stress was due to the reduction of internal stresses pre-existing within the deformation twins. The complete reduction of internal stresses at about 530 degrees C led to the equivalence of the critical stresses of different detwinning modes and a decrease in the yield stress anisotropy of the twin/matrix structure.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Nature of the electric double layer to modulate the electrochemical behaviors of Fe2O3 electrode

Taowen Dong, Tingting Qin, Wei Zhang, Yaowen Zhang, Zhuoran Feng, Yuxiang Gao, Zhongyu Pan, Zixiang Xia, Yan Wang, Chunming Yang, Peng Wang, Weitao Zheng

Summary: The interaction between the electrode and the electric double layer (EDL) significantly influences the energy storage mechanism. By studying the popular alpha-Fe2O3 electrode and the EDL interaction, we find that the energy storage mechanism of the electrode can be controlled by modulating the EDL.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Grain scale bursts of plasticity in Mg-4Zn via high energy X-rays: Towards twin observation in real-time

Matthew R. Barnett, Jun Wang, Sitarama R. Kada, Alban de Vaucorbeil, Andrew Stevenson, Marc Fivel, Peter A. Lynch

Summary: The elastic-plastic transition in magnesium alloy Mg-4.5Zn exhibits bursts of deformation, which are characterized by sudden changes in grain orientation. These bursts occur in a coordinated manner among nearby grains, with the highest burst rate observed at the onset of full plasticity. The most significant burst events are associated with twinning, supported by the observation of twinned structures using electron microscopy. The bursts are often preceded and followed by a stasis in peak movement, indicating a certain "birth size" for twins upon formation and subsequent growth at a later stage.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Atomistic simulations and machine learning of solute grain boundary segregation in Mg alloys at finite temperatures

Vaidehi Menon, Sambit Das, Vikram Gavini, Liang Qi

Summary: Understanding solute segregation thermodynamics is crucial for investigating grain boundary properties. The spectral approach and thermodynamic integration methods can be used to predict solute segregation behavior at grain boundaries and compare with experimental observations, thus aiding in alloy design and performance control.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Integrating abnormal thermal expansion and ultralow thermal conductivity into (Cd,Ni)2Re2O7 via synergy of local structure distortion and soft acoustic phonons

Feiyu Qin, Lei Hu, Yingcai Zhu, Yuki Sakai, Shogo Kawaguchi, Akihiko Machida, Tetsu Watanuki, Yue-Wen Fang, Jun Sun, Xiangdong Ding, Masaki Azuma

Summary: This study reports on the negative and zero thermal expansion properties of Cd2Re2O7 and Cd1.95Ni0.05Re2O7 materials, along with their ultra-low thermal conductivity. Through investigations of their structures and phonon calculations, the synergistic effect of local structure distortion and soft phonons is revealed as the key to achieving these distinctive properties.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

Semi-automatic miniature specimen testing method to characterize the plasticity and fracture properties of metals

Thomas Beerli, Christian C. Roth, Dirk Mohr

Summary: A novel testing system for miniature specimens is designed to characterize the plastic response of materials for which conventional full-size specimens cannot be extracted. The system has an automated operation process, which reduces the damage to specimens caused by manual handling and improves the stability of the test results. The experiments show that the miniature specimens extracted from stainless steel and aluminum have high reproducibility, and the results are consistent with those of conventional-sized specimens. A correction procedure is provided to consider the influence of surface roughness and heat-affected zone caused by wire EDM.

ACTA MATERIALIA (2024)

Article Materials Science, Multidisciplinary

The effect of microstructure and film composition on the mechanical properties of linear antenna CVD diamond thin films

Rani Mary Joy, Paulius Pobedinskas, Nina Baule, Shengyuan Bai, Daen Jannis, Nicolas Gauquelin, Marie-Amandine Pinault-Thaury, Francois Jomard, Kamatchi Jothiramalingam Sankaran, Rozita Rouzbahani, Fernando Lloret, Derese Desta, Jan D'Haen, Johan Verbeeck, Michael Frank Becker, Ken Haenen

Summary: This study investigates the influence of film microstructure and composition on the Young's modulus and residual stress in nanocrystalline diamond thin films. The results provide insights into the mechanical properties and intrinsic stress sources of these films, and demonstrate the potential for producing high-quality nanocrystalline diamond films under certain conditions.

ACTA MATERIALIA (2024)