4.6 Article

Surfactantless synthesis of Fe3O4 magnetic nanobelts by a simple hydrothermal process

Journal

MATERIALS LETTERS
Volume 75, Issue -, Pages 172-174

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2012.02.029

Keywords

Nanoparticles; Magnetic materials; Fe3O4 nanobelts; FeCl2

Funding

  1. National Natural Science Foundation of China [51106061, 21106051, 20975043]
  2. Natural Science Foundation of Jiangsu Education Committee [10KJB430003]
  3. Technological Research Foundation of Huai'an City [HAG2010073]
  4. Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials [JSKC11095]

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Fe3O4 nanobelts were prepared by a surfactantless hydrothermal process. FeCl2 and Na2CO3 were used as iron and alkali sources, respectively. X-ray diffraction and energy dispersive spectroscopy showed that the as-prepared product was pure cubic-phase Fe3O4 without any impurity. Scanning electron microscopy and transmission electron microscopy indicated that the Fe3O4 nanobelts had lengths of 400 to 1500 nm and widths of 80 to 120 nm. Investigations on the effects of other iron and alkali sources on the Fe3O4 nanostructures indicated that both FeCl2 and Na2CO3 were indispensable to the formation of Fe3O4 nanobelts. Magnetic analysis revealed that the Fe3O4 nanobelts had ferromagnetic behavior with a saturation magnetization of 74.54 emu g(-1). (C) 2012 Elsevier B.V. All rights reserved.

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