Journal
MATERIALS LETTERS
Volume 64, Issue 21, Pages 2302-2305Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2010.07.043
Keywords
Oligo(o-phenylenediamine); NaClO2; Self-assembly; Microfibers
Funding
- National Science Foundation for Distinguished Young Scholars [50925417]
- National Natural Science of China [50830301]
- National Key Technology RD Program [2007BAC25B01]
- Ministry of Education of China [308019]
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Oligo(o-phenylenediamine) (OoPD) microfibers were successfully synthesized in acidic solution by mixing o-phenylenediamine (oPD) and NaClO2 solutions together. As proved by the mass spectroscopy (MS), 1H nuclear magnetic resonance spectroscopy (H-1 NMR) and Fourier transform infrared spectroscopy (FTIR), the OoPD is composed of 2,3-diaminophenazine and 2,2'-diaminoazobenzene. Based on the scanning electron microscopy (SEM), these microfibers were observed to be rigid and smooth. However, the smooth microfibers became the saw-like materials when pH value of oPD solution increased. The method used is facile and large-scale. (C) 2010 Elsevier B.V. All rights reserved.
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