Journal
MATERIALS & DESIGN
Volume 35, Issue -, Pages 276-280Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.matdes.2011.09.032
Keywords
Composites; Microstructure; Electrical
Categories
Funding
- PhD Programs Foundation of Shandong Province of China [BS2010CL010]
- Natural Science Foundation of Shandong Province of China [ZR2 011EMQ015]
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Gd2O3 (0-0.8 wt.%)-doped 0.82Bi(0.5)Na(0.5)TiO(3)-0.18Bi(0.5)K(0.5)TiO(3) (BNKT18) lead-free piezoelectric ceramics were synthesized by a conventional solid-state process. The effects of Gd2O3 on the microstructure, the dielectric, ferroelectric and piezoelectric properties were investigated. X-ray diffraction (XRD) data shows that Gd2O3 in an amount of 0.2-0.8 wt.% can diffuse into the lattice of BNKT18 ceramics and form a pure perovskite phase. Scanning electron microscope (SEM) images indicate that the grain size of BNKT18 ceramics decreases with the increase of Gd2O3 content; in addition, all the modified ceramics have a clear grain boundary and a uniformly distributed grain size. At room temperature, the ferroelectric and piezoelectric properties of the BNKT18 ceramics have been improved with the addition of Gd2O3, and the BNKT18 ceramics doped with 0.4 wt.% Gd2O3 have the highest piezoelectric constant (d(33) = 137 pC/N), highest relative dielectric constant (epsilon(r) = 1023) and lower dissipation factor (tan delta = 0.044) at a frequency of 10 kHz. The BNKT18 ceramics doped with 0.2 wt.% Gd2O3 have the highest planar coupling factor (k(p) = 0.2463). (C) 2011 Elsevier Ltd. All rights reserved.
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