4.4 Article

Improvement of Energy Dispersive X-Ray Fluorescence Throughput: Influence of Measuring Times and Number of Replicates on Validation Performance Characteristics

Journal

FOOD ANALYTICAL METHODS
Volume 3, Issue 2, Pages 104-115

Publisher

SPRINGER
DOI: 10.1007/s12161-009-9101-4

Keywords

EDXRF; Measuring Time; Replicates; Validation; Performance

Ask authors/readers for more resources

The mineral nutrients Na, Mg, P, Cl, K, Ca, Fe, and Zn are commonly quantified by X-ray fluorescence energy dispersive (EDXRF) and wavelength dispersive systems in food matrices such as milk-and cereal-based powders in order to ensure their quality control. In order to optimize EDXRF use on production sites as well as in research and development laboratories, the influence of the number of pellets per sample and the measuring time has been investigated. The results obtained were systematically compared to data obtained by reference analytical methods (inductively coupled plasma-atomic emission spectrometry and potentiometry). A methodology based on statistical comparison of validation performance characteristics, obtained on a recent commercial instrument, is proposed.

Authors

I am an author on this paper
Click your name to claim this paper and add it to your profile.

Reviews

Primary Rating

4.4
Not enough ratings

Secondary Ratings

Novelty
-
Significance
-
Scientific rigor
-
Rate this paper

Recommended

No Data Available
No Data Available