Journal
FARADAY DISCUSSIONS
Volume 170, Issue -, Pages 35-40Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4fd00006d
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We employ vortex grinding to generate a [2.2] paracyclophane in the organic solid state. The vortex grinding is aided with the addition of a small amount of liquid phase to facilitate topochemical [2 + 2] photodimerizations that generate the cyclophane stereoselectively and in up to quantitative yield. The use of the liquid phase increases the scope of the vortex method.
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