Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2014, Issue 7, Pages 1541-1546Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201301561
Keywords
N-Arylation; Cross-coupling; Copper; Ligand-free reactions; Sulfonamides
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Funding
- National Institute of Education, Singapore
- Nanyang Technological University
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A simple and practical protocol for the cross-coupling of methanesulfonamide and aryl iodides under ligand-free copper(I)-oxide-catalyzed conditions in water is reported. The method allows the preparation of a wide variety of synthetically useful N-arylated methanesulfonamides in good to excellent yields (up to 90%) under the optimized conditions.
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