Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2013, Issue 19, Pages 4156-4162Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201201731
Keywords
Synthetic methods; Acylation; Microwave chemistry; Peptides; Conjugates
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Funding
- University of Florida
- Kenan Foundation
- King Abdulaziz University, Jeddah, Saudi Arabia
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(alpha-Benzyloxycarbonyl-aminoacyl)benzotriazolides (Cbz = benzyloxycarbonyl) underwent a coupling reaction with -hydrazino acids under microwave irradiation to form hybrid hydrazino dipeptides (42-71%). Chiral acylations of -N-Cbz--hydrazino acylbenzotriazolides were successfully carried out with N-, S-, O-, and C-nucleophiles in yields of 49-88%.
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