Journal
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
Volume -, Issue 22, Pages 3473-3477Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejic.201000043
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Funding
- National Nature Science Foundation of China (NSFC) [20871027, 20973035]
- Program for New Century Excellent Talents in University [NCET-07-0169]
- Program for Changjiang Scholars and Innovative Research Team in University
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The dimeric, zirconium-sandwiching compound K4H6[Zr-4-(OH)(6)(CH3COO)(2)(alpha-PW10O37)(2)]center dot 23H(2)O (1) was obtained by the reaction of lacunary [PW11O39](7-) and ZrCl4 in a 1 M potassium acetate buffer. It was characterized by elemental and thermogravimetric analysis, X-ray crystallography, solution W-183 NMR, FTIR, and UV spectroscopy, and cyclic voltammetry (CV). All the studies indicate that compound 1 is stable both in the solid state and in solution. The cyclic voltammograms indicate good electrocatalytic activity in the reduction of nitrite.
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