Journal
ELECTRONIC MATERIALS LETTERS
Volume 8, Issue 2, Pages 209-213Publisher
KOREAN INST METALS MATERIALS
DOI: 10.1007/s13391-012-2037-7
Keywords
solid electrolyte; all-solid-state; lithium ion battery; sulfide; mechanical milling
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Funding
- Fundamental R&D Program for Core Technology of Materials
- Korean Ministry of Knowledge Economy [10037233]
- Korea Evaluation Institute of Industrial Technology (KEIT) [10037233, 10037276] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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In order to improve the performance of all-solid-state batteries, 78Li(2)S.22P(2)S(5) glass-ceramics with an enhanced ionic conductivity of 8.5 x 10(-4) S cm(-1) were developed using a two-step heat treatment after mechanical milling. The two-step heat treatment process consists of a nucleation step at 160 degrees C and a crystal growth step at 230 degrees C, where the nucleation temperature was determined using previously performed thermal analyses. Moreover, the wet mixing method, which is identified as an effective method of obtaining more homogeneous distributions of composite particles, was applied in order to prepare the composite cathode. As a result, the cell prepared using the wet mixing method exhibited significantly improved capacity retention.
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