Journal
ELECTROCHEMISTRY COMMUNICATIONS
Volume 11, Issue 12, Pages 2261-2264Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.elecom.2009.09.040
Keywords
Methylene blue; N,N-dimethyl-p-phenylenediamine; Cyclic voltammetry; Electrochemical synthesis; Michael-type reaction
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An efficient and one-pot electrochemical method for the synthesis of methylene blue based on the Michael-type reaction of electrochemically generated quinone-diimine derived from oxidation of N,N-dimethyl-p-phenylenediamine in the presence of sodium sulfide as nucleophile in aqueous solution via EC-ECECC mechanism is reported. (C) 2009 Elsevier B.V. All rights reserved.
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