Journal
ELECTROANALYSIS
Volume 24, Issue 1, Pages 101-106Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.201100436
Keywords
Adsorptive stripping voltammetry; Lead film electrode; Acidic medium; Tungsten analysis
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Funding
- Foundation for Polish Science (START)
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For the first time an in situ plated lead film electrode was applied to adsorptive stripping voltammetry at relatively strong acidic conditions of, e.g., pH 2. As an example of the application of such electrode a procedure for ultratrace W(VI) determination by adsorptive stripping voltammetry was elaborated. The procedure is based on the preconcentration of the W(VI)-Alizarin Red S complex at an in situ plated lead film electrode held at -0.575 V (vs. Ag/AgCl), followed by a negatively sweeping square wave voltammetric scan. The proposed voltammetric procedure was applied to W(VI) determination in natural water samples.
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