Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 5, Pages 2925-2929Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b00167
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Funding
- National Natural Science Foundation of China [21272117]
- Priority Academic Program Development of Jiangsu Higher Education Institutions
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An efficient synthesis of phenols via Pd-catalyzed, pyridyl-directed homogeneous hydroxylation of the aryl C-H bond was developed, in which tert-butyl hydroperoxide was used as the sole oxidant. The method had a broad group tolerance and was available for both electron-rich and electron-deficient substrates. The reaction of a series of 2-arylpyridine derivatives gave the ortho-hydroxylation products in moderate to good yields.
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