Journal
DALTON TRANSACTIONS
Volume 43, Issue 13, Pages 4945-4949Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3dt53589d
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Funding
- Swiss National Science Foundation [PA00P2-145308]
- ERC [247450]
- EPSRC [EP/F034210/1]
- EC COST Action [CM1105]
- University of Warwick of the solid state NMR infrastructure at Warwick
- Advantage West Midlands (AWM)
- European Regional Development Fund (ERDF)
- Swiss National Science Foundation (SNF) [PA00P2_145308] Funding Source: Swiss National Science Foundation (SNF)
- EPSRC [EP/F034210/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/F034210/1] Funding Source: researchfish
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The first H-1, C-13, P-31 and B-11 solid state MAS NMR studies of electron- deficient carborane-containing ruthenium and osmium complexes [Ru/Os(p-cym)(1,2-dicarba-closo-dodecaborane-1,2-dithiolate)] are reported. The MAS NMR data from these 16-electron complexes are compared to those of free carborane-ligand and an 18-electron triphenylphosphine ruthenium adduct, and reveal clear spectral differences between 16- and 18-electron organometallic carborane systems in the solid state.
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