Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 85, Pages 10010-10012Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc45349a
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The direct reduction of carboxylic acids to disilylacetals was achieved through a manganese catalyzed hydrosilylation reaction in the presence of triethylsilane under mild conditions, at r.t. and under UV irradiation (350 nm). The aldehydes were obtained in good to excellent yields after acidic hydrolysis.
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