Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 45, Pages 5150-5152Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc42160k
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Funding
- Leverhulme Trust
- EPSRC
- Engineering and Physical Sciences Research Council [1093835] Funding Source: researchfish
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The scope of the asymmetric silyl transfer to unsaturated lactones utilising a C-2-symmetric NHC-Cu(I) catalyst has been established and kinetic resolutions mediated by silyl transfer have been used to prepare enantiomerically enriched anti-4,5-disubstituted 5-membered lactones. The method has been exploited in an expedient synthesis of (+)-blastmycinone.
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