Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 14, Pages 2024-2026Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc17616e
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Funding
- National Natural Science Foundation of China [20872073, 21150110105, 21172125]
- Ministry of Education of China [B06005]
- Committee of Science and Technology of Tianjin
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An iron(III)-catalyzed three-component coupling reaction of alkynes, CH2Cl2 and amines was developed for facile synthesis of propargylamines. Preliminary mechanism investigation using in situ FT-IR reveals that the crucial Fe-acetylide intermediate could be formed through C-H bond activation of alkynes thanks to cooperative effect of FeCl3 and 1,1,3,3-tetramethylguanidine.
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