Journal
CHEMICAL COMMUNICATIONS
Volume -, Issue 27, Pages 3172-3174Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b802043d
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A water-compatible Pd(II) pincer with a hybrid [SNS]-donor set, [(LPdCl)-Pd-1]Cl center dot 2H(2)O [L-1=bis-(2-(i-butylsulfanyl)-ethyl)-amine] has been isolated and crystallographically characterized; its solid lattice at 223 K contains a ladder-like water polymer of tetramers and extensive H-bonding exists among the cation, anion and water cluster, and this water-soluble complex is active in Suzuki-Miyaura coupling of phenylboronic acid and selected aryl bromides in water at 75 degrees C.
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