4.7 Article

Mechanical properties and consolidation of binderless nanostructured (Ti,Cr)C from mechanochemically-synthesized powder by high-frequency induction heating sintering

Journal

CERAMICS INTERNATIONAL
Volume 39, Issue 8, Pages 9721-9726

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2013.04.053

Keywords

Sintering; Fracture toughness; Mechanical properties; Nanostructured material; Powder metallurgy

Funding

  1. Korea Institute of Geoscience and Mineral Resources (KIGAM)
  2. Ministry of Knowledge Economy of Korea
  3. Human Resources Development of the Korea Institute of Energy Technology Evaluation and Planning (KETEP)
  4. Korea Government Ministry of Knowledge Economy [20114030200060]
  5. National Research Council of Science & Technology (NST), Republic of Korea [13-3111-1.2.3] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)

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Solid-solution nanocrystalline powder, (Ti,Cr)C, was prepared via high-energy milling of Ti alloys with graphite resulting in the B1 structure (NaCl-like structure) phase. The synthesis process was investigated in terms of the phase evolution by analyzing XRD data. The rapid sintering of nanostuctured hard (Ti,Cr)C materials was performed by a high-frequency induction-heating sintering process. This process allows quick densification to near theoretical density and inhibits grain growth. A dense, nanostructured (Ti,Cr)C hard material with a relative density of up to 97% was produced by simultaneous application of 80 MPa and an induced current of 15 kW for 2 min. The microstructure and mechanical properties of the resulting binderless (Ti,Cr)C were investigated. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

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