Journal
CATALYSIS LETTERS
Volume 142, Issue 1, Pages 81-86Publisher
SPRINGER
DOI: 10.1007/s10562-011-0708-x
Keywords
Formaldehyde; Carbonylation; Methyl glycolate; Ethylene glycol; Ionic liquids
Categories
Funding
- National Basic Research Program of China (973 Program) [2011CB201404]
- Key Project of the National Twelfth-Five Year Research Program of China [2011BAE17B00]
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Methyl glycolate (MG), as a precursor to ethylene glycol (EG), was synthesized by an efficient and eco-friendly procedure of one-pot, two-step, sequential reaction, including carbonylation and esterification from HCHO with Bronsted acidic ionic liquids (BAILs) as catalysts. MG was obtained in high yield under mild conditions. In addition, the catalyst could be recycled eight times after separating the unreacted materials and products from the reaction system by distillation under vacuum and no significant decrease in catalytic activity was observed.
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