Journal
CARBOHYDRATE RESEARCH
Volume 379, Issue -, Pages 26-29Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2013.06.009
Keywords
Bacterial oligosaccharides; Glycosylation; H2SO4-silica
Funding
- UGC, New Delhi
- DST, New Delhi, India [SR/FTP/CS-110/2005]
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Chemical synthesis of the trisaccharide repeating unit of the O-polysaccharide from Aeromonas hydrophila A19 (O:14) is reported in the form of its p-methoxyphenyl glycosides. Suitably protected monosaccharide synthons were prepared either by literature procedure or by strategies developed in house. Stereoselective glycosylations were accomplished by the activation of thioglycosides using N-iodosuccinimide in conjunction with H2SO4-silica in good to excellent yields. (C) 2013 Elsevier Ltd. All rights reserved.
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