Journal
BULLETIN OF THE KOREAN CHEMICAL SOCIETY
Volume 32, Issue 5, Pages 1583-1586Publisher
KOREAN CHEMICAL SOC
DOI: 10.5012/bkcs.2011.32.5.1583
Keywords
Silver nanoparticles; Ionic liquids; Nanodroplets
Categories
Funding
- Priority Research Centers Program [2009-0093829]
- Ministry of Education, Science and Technology [R31-10069]
- IBST of Dankook University
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Silver nanoparticles (< 10 nm) were prepared in ultrasonic vibration-induced nanodroplets of isopropyl alcohol (IPA) in combination with hydrophobic room temperature ionic liquids (RTILs). The Ag-precursor used were silver (I) complex, Ag(2)(ehac)(2)(eha)(2) (ehac = 2-ethylhexylammonium carbamate; eha = 2-ethylhexylamine), in IPA, while 1-butyl-3-methylimidazolium-based ionic liquids bearing SbF(6)(-), PF(6)(-) and NTf(2)(-) as counter anions were used as RTILs. During sonication for 10-90 min at room temperature, uniform silver nanoparticles with mean sizes of 2 to 8 nm were rapidly synthesized. Transmission electron micrographs also confirmed that silver nanoparticles have a spherical shape and diverse sizes depending on the reaction time (10-90 min).
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