Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 7, Issue -, Pages 740-743Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.7.84
Keywords
clavukerin A; cycloisomerization; gold catalyst; hydrogenation; stereoselectivity
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Funding
- National Research Foundation [NRF-2007-0052533, NRF-331-2008-1-C00165]
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An efficient formal total synthesis of (+/-)-clavukerin A was accomplished via a gold-catalyzed cycloisomerization of a 3-methoxy-1,6-enyne 5 as the key strategy followed by Rh-catalyzed stereoselective hydrogenation of the cycloheptenone 4.
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