Journal
ARABIAN JOURNAL FOR SCIENCE AND ENGINEERING
Volume 39, Issue 1, Pages 563-568Publisher
SPRINGER HEIDELBERG
DOI: 10.1007/s13369-013-0879-4
Keywords
Green synthesis; Electrolysis decomposition; Tea extract
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In the present work, green synthesis of silver nanoparticles is investigated. The process is simple, environmentally friendly, cheaper and efficient. Instead of hazardous chemicals, Tea extract was used as a capping agent. In this process, electrolytic deposition of silver nanoparticles is done on a carbon rod wrapped with low-density polyethylene (LDPE). It was found that the current flowing in the circuit controls the size of the nanoparticles. A DC source was applied across the electrodes placed in a very dilute solution of AgNO3(0.01N), continuously magnetically stirred, over a period of 48 h at room temperature (30 A degrees C). The as-synthesized silver nanoparticles were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and UV-vis spectroscopy. XRD patterns reveal that face-centered cubic structured silver particles were synthesized and the interplanar d-spacing of the corresponding lines presented in the powder XRD pattern match those of standard JCPDS file no. 04-0783. TEM analysis shows that silver nanoparticles of spherical and oval shape were synthesized. The particle size of the as-synthesized nanoparticles ranged from 5 to 100 nm for different values of current. The UV-vis spectroscopy shows the absorbance in visible range. As the particle size increases the absorption shifts towards higher wavelength region.
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