4.7 Article

Preparation and characterization of polyacrylamide/palygorskite

Journal

APPLIED CLAY SCIENCE
Volume 46, Issue 2, Pages 148-152

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.clay.2009.07.018

Keywords

Acrylamide; Grafting; Mercury; Adsorption; Palygorskite; Silane coupling agents

Funding

  1. National Natural Science Foundation of China [20776067]
  2. Natural Science Foundation of Jiangsu Education Department [07KJA15012, 08KJD530002, 07KJD150025]
  3. Program for Science and Technology Development of Huaian [HAG08041]

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Polyacrylamide/palygorskite(PAM/PA) as prepared by solution polymerization of acrylamide (AM) oil the gamma-methacryloxypropyl trimethoxy-silane (KH-570) modified palygorskite (PA). The influence of monomer concentration, polymerization time, initiator concentration and polymerization temperature on mercury adsorption of PAM/PA was investigated. The maximum adsorption capacity was 135.5 mg/g at optimum polymerization conditions. PAM/PA was characterized by thermogravimetric analysis (TGA), differential scanning calorimetry (DSC). Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) (C) 2009 Elsevier B.V. All rights reserved.

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