4.5 Article

Crystallisation kinetics of hydroxyapatite thin films prepared by sol-gel process

Journal

ADVANCES IN APPLIED CERAMICS
Volume 109, Issue 6, Pages 313-317

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1179/174367609X422144

Keywords

Sol-gel chemistry; Nanostructures; Thin films; Hydroxyapatit

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In this study, the crystallisation of nano hydroxyapatite ( HA) films on stainless steel 316L was studied. The film was prepared by sol-gel technique. The process was started with preparation of an HA sol. After aging of the sol at room temperature, a stainless steel 316L substrate was dip coated and then was heat treated from 350 to 450 degrees C at different periods of time in air. The crystallisation behaviour and the transformation-temperature-time diagram of HA films were achieved and analysed using the avrami equation. The results showed that the crystallisation of HA began at 250 degrees C and was increased up to 450 degrees C. The obtained HA film showed a nanostructure character with a suitable crystalinity after heat treatment.

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