Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 356, Issue 7, Pages 1625-1630Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201300999
Keywords
catechol; CH hydroxylation; palladium; ruthenium; weak coordination
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Funding
- Ministry of Science and Technology [2011CB965300]
- National Natural Science Foundation of China [21302106]
- Tsinghua University Initiative Scientific Research Program
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An efficient ruthenium(II)- and palladium(II)-catalyzed CH hydroxylation of aryl carbamates has been developed for the facile synthesis of catechols and pyrogallols. The reaction demonstrates excellent reactivity, regio- and chemoselectivity, good functional group compatibility and high yields. The practicality of this method has been proved by a gram-scale synthesis.
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