Journal
CHEMPLUSCHEM
Volume 83, Issue 1, Pages 42-46Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cplu.201700440
Keywords
3D printing; acylation; flexible microfluidic devices; flow synthesis; microwave chemistry
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A large-area, all-flexible, microwaveable polydimethoxysilane microfluidic reactor was fabricated by using a 3D printing system. The sacrificial microchannels were printed on polydimethoxysilane substrates by a direct ink writing method using water-soluble Pluronic F-127 ink and then encapsulated between polydimethoxysilane layers. The structure of micron-sized channels was analyzed by optical and electron microscopy techniques. The fabricated flexible microfluidic reactors were utilized for the acetylation of different amines under microwave irradiation to obtain acetamides in shorter reaction times and good yields by flow organic synthesis.
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