Journal
TETRAHEDRON LETTERS
Volume 59, Issue 13, Pages 1200-1203Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2018.02.024
Keywords
Iron(III) chloride; Iron(III) bromide; alpha-Halomethyl ketone; alpha-Diazo-ketones; Silica gel
Categories
Funding
- NSFC [21372056, 21642011, 81573529]
- Changjiang Scholars and Innovative Research Team in Chinese University [IRT 1231]
- Hangzhou Normal University [2012QDL001]
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An efficient and mild method for the synthesis of alpha-halomethyl ketones from a-diazo ketones was developed using ferric chloride or bromide as the halogen source and silica gel as the hydrogen source, with good to excellent yields. (C) 2018 Elsevier Ltd. All rights reserved.
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