Journal
SYNTHETIC COMMUNICATIONS
Volume 48, Issue 3, Pages 278-284Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2017.1397697
Keywords
Amidation; boron dipyrromethene (BODIPY); hydrogenolysis; N-hydroxysuccinimide ester; tripod
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Funding
- Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD)
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A novel tripod boron dipyrromethene (BODIPY) dye bearing N-hydroxysuccinimide ester was synthesized through its carboxylic acid precursor, and the functionality was confirmed by its amidation reaction with a primary amine. It is the first time that a reactive functional group was introduced onto a tripod BODIPY structure. All the new structures had been characterized by NMR, HRMS, and IR spectra. The introduction of an electron-donative diethylamine proved to be a key factor for the successful hydrogenolysis of the corresponding tris-substituted 1,3,5-triazine structure. [GRAPHICS] .
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