Journal
SYNTHESIS-STUTTGART
Volume 50, Issue 7, Pages 1560-1568Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1591746
Keywords
C-glycosylation; 2-naphthols; Lewis acids; trichloroacetimidate; glycosyl donors; substituent effects
Categories
Funding
- CSIR
- Council of Scientific and Industrial Research (CSIR) [02(0183)/14/EMRII]
- IIT Kharagpur
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Several glycosyl donors have been systematically investigated for C-glycosylation of substituted -naphthols to delineate the effect of the substituents. Whereas glycosylations of the parent 2-naphthol are smoothly achievable, those of differently substituted 2-naphthols are cumbersome. Efficiency of the glycosylation depends on the nature of both the glycosyl donors and the substituents of the arene ring. Among various glycosyl donors, trichloroacetimidate glycosyl donors are found to be superior for glycosylation with substituted 2-naphthols.
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