Journal
ORGANIC LETTERS
Volume 20, Issue 15, Pages 4571-4574Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b01761
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Funding
- National Natural Science Foundation of China [21562005, 21602037]
- Natural Science Foundation of Guangxi [2015GXNSFCA139001, 2016GXNSFFA380005]
- Ministry of Education [IRT_16R15]
- Overseas 100 Talents Program of Guangxi Higher Education
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Various benzoxazonines were synthesized through a formal [7 + 2] cycloaddition of arynes with N-vinyl-alpha,beta-unsaturated nitrones under mild conditions. Controllable N-O bond cleavage of benzoxazonines afforded polysubstituted pyrrole-tethered benzopyrans and acyclic ketone-substituted phenols in moderate to good yields. Further transformations provided a facile approach to access useful building blocks with specific stereoselectivity.
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