4.5 Article

Use of an Annular Silicon Drift Detector (SDD) Versus a Conventional SDD Makes Phase Mapping a Practical Solution for Rare Earth Mineral Characterization

Journal

MICROSCOPY AND MICROANALYSIS
Volume 24, Issue 3, Pages 238-248

Publisher

CAMBRIDGE UNIV PRESS
DOI: 10.1017/S1431927618000417

Keywords

annular silicon drift detector; field emission scanning electron microscope; phase map; rare earth minerals; X-ray microanalysis

Funding

  1. NSERC
  2. Avalon through the Collaborative Research and Development Grant program [CRDPJ-445372-12]
  3. McGill Engineering Doctoral Awards (MEDA)

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A number of techniques for the characterization of rare earth minerals (REM) have been developed and are widely applied in the mining industry. However, most of them are limited to a global analysis due to their low spatial resolution. In this work, phase map analyses were performed on REM with an annular silicon drift detector (aSDD) attached to a field emission scanning electron microscope. The optimal conditions for the aSDD were explored, and the high-resolution phase maps generated at a low accelerating voltage identify phases at the micron scale. In comparisons between an annular and a conventional SDD, the aSDD performed at optimized conditions, making the phase map a practical solution for choosing an appropriate grinding size, judging the efficiency of different separation processes, and optimizing a REM beneficiation flowsheet.

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