Journal
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
Volume 165, Issue 7, Pages H399-H406Publisher
ELECTROCHEMICAL SOC INC
DOI: 10.1149/2.1121807jes
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Electrochemically deposited polymeric film of polyaniline (PANT) is used as a substrate for electrochemical deposition of platinum by using cyclic voltammetry. The electrochemical properties of multi-layered films were analyzed by cyclic voltammetry and AC impedance spectroscopy. The structural properties of multi-layered polymer films were analyzed by SEM, TEM, XRD, XPS, Raman and FTIR. The modified electrode showed strong electrocatalytic activity toward oxidation of toluene in presence of NaNO2/H2SO4 in actetonitrile medium. Toluene gave a sensitive anodic peak at 1.318 V (vs. SCE). Cyclic voltammetry studies suggest that the electrochemical activity of Pt-PANT/CFP electrode is higher than that of Pt/CFP electrode toward toluene oxidation. (C) 2018 The Electrochemical Society.
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