Journal
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY
Volume 95, Issue 1, Pages 13-19Publisher
WILEY
DOI: 10.1002/aocs.12010
Keywords
Sesame oil; Lignan; -Tocopherol; Normal phase liquid chromatography
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Funding
- National Natural Science Foundation of China [31401525]
- China Postdoctoral Science Foundation [2015M571666]
- Shandong Province Postdoctoral Science Foundation [145635]
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A novel method for rapid and simultaneous analysis of three lignans and -tocopherol in sesame oil has been established based on a one-step solvent extraction followed by normal-phase liquid chromatography. The briefness of the experimental procedure, use of 5mL of n-hexane/isopropanol (98:2, v/v) for extraction without any further cleanup process, short analysis time (10 min), and excellent sensitivity and selectivity demonstrated the advantages of this practical and efficient method. All the analytes exhibited satisfactory recoveries ranging from 95.4 to 103.4% at three spiked levels, with the relative SD ranging from 1.1 to 4.4%. The limits of quantitation of this method for four analytes were in the range of 0.3-1.0 gg(-1). The validated method was successfully applied to the coinstantaneous determination of lignan and -tocopherol in five real sesame oil samples. Furthermore, the results of this study were compared with previously reported method and standard method.
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