Journal
INTERNATIONAL JOURNAL OF ELECTROCHEMICAL SCIENCE
Volume 13, Issue 6, Pages 5681-5697Publisher
ESG
DOI: 10.20964/2018.06.66
Keywords
AZ91 Mg alloy; plasma-electrolytic-oxidation (PEO) coating; Y2O3 nanoparticle; corrosion resistance; microhardness
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Funding
- Ground Plan of Science and Technology Projects of Jiangxi Province [KJLD2013078]
- Open Project of the Jiangxi Provincial Engineering Research Center for Magnesium Alloys [2017]
- Innovation and Entrepreneurship Training Program for College Students of Gannan Normal University [201766]
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Yttrium oxide (Y2O3) nanoparticles were added to the electrolyte during the preparation of a plasmaelectrolytic-oxidation (PEO) coating on the AZ91 Mg alloy. The effects of the Y2O3 nanoparticles on the microstructure, phase components, chemical compositions, and mechanical properties of the PEO coating were investigated by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and microhardness tests. Furthermore, the corrosion resistance of the PEO coating was evaluated by pote ntiodynamic polarization curves and electrochemical impedance spectroscopy (EIS). The results indicated that the Y2O3 nanoparticles had been incorporated into the PEO coating and that the number of micropores and cracks in the coating was dramatically decreased. The microhardness of the PEO coating was more than 10 times higher than that of the AZ91 Mg substrate, and the corrosion current density decreased by approximately three orders of magnitude when 3 g/L of Y2O3 nanoparticles was added to the corresponding electrolyte.
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